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China Journal of Chinese Materia Medica ; (24): 2118-2121, 2008.
Article in Chinese | WPRIM | ID: wpr-252187

ABSTRACT

<p><b>OBJECTIVE</b>To study the chemical constituents from the ethyl acetate portion of an ethanolic extractive of the leaves of Aeschynanthus mengxinensis.</p><p><b>METHOD</b>The column chromatographic techniques were applied to isolate constituents. A combination of IR, ESI-MS, NMR and 2D-NMR spectroscopy was used to identify structures.</p><p><b>RESULT</b>Four compounds were isolated from the ethyl acetate fraction of this plant, and the structure of them have identified as 2alpha, 3beta, 19beta-trihydroxyolean-12-ene-23,28-dioic acid (1), 2alpha, 3beta, 21beta-trihydroxyolean-12-ene-28-oic acid (2), 2alpha, 3beta, 23-trihydroxyurs-12-ene-28-oic acid (3) and stigmast-5 (6), 22 (23)-diene-3beta-ol (4).</p><p><b>CONCLUSION</b>The NMR data of compound 1 was completely assigned by 2D-NMR techniques, including HMBC and HMQC. Compounds 1-4 were isolated for the first time from Gesneriaceae.</p>


Subject(s)
Drugs, Chinese Herbal , Chemistry , Magnoliopsida , Chemistry , Plant Leaves , Chemistry , Terpenes , Chemistry
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