ABSTRACT
Aims: The aims of this study were to investigate batch-to-batch differences in mechanical and thermal properties of 22 commercial nickel-titanium wires and evaluate the surface quality. Secondly the percentages of superelasticity at mouth temperature were measured. Study Design: In vitro laboratory study. Place and Duration of Study: Sample: Department of Oral Health Sciences – Orthodontics and Metallurgy and Materials Engineering KU Leuven, between January 2010 and May 2011. Methodology: The sample comprised 22 NiTi wires of the upper jaw from 7 different manufacturers. For each brand two different batches were investigated (LOT A, LOT B). Three different investigations were carried out. First transformation behaviour and transition temperatures were determined by differential scanning calorimetry, second a three point bending test was done to evaluate the mechanical properties and third scanning electron microscopy was performed on all samples to evaluate surface quality. Results: Absolute batch-to-batch differences in the investigated properties were all deviating from zero, although most differences were clinically acceptable. Significant interbatch differences in thermal properties were found in 4 wires. Mechanical interbatch differences were found remarkable for 5 wires. Percentage of elasticity showed a non- superelastic curve below a deflection of 1500 μm, which represents clinical small deflections. Surface topography showed also interbatch differences for 4 wires. Conclusion: This study shows that batch-to-batch differences are obvious in each sample. One has to be careful in the selection of archwires. Therefore more standardized consument information should be provided.
ABSTRACT
The purpose of this study was to investigate the change of 3 point bending properties of various nickel titanium wires after recycling. Four types of nickel-titanium (Align: martensitic type, NiTi, Optimalloy, Sentalloy: austenitic type) wires were divided to three groups: as-received condition (T0: control group), treated in artificial saliva for four weeks (T1) and autoclaved after being treated in artificial saliva (T2). Detrimental changes were observed for the selected mechanical properties in three point bending test. Loading force at 3mm deflection, unloading force at 3mm deflection, stress hysteresis, loading force at 1mm deflection, unloading force at 1 mm deflection and stress hysteresis at 1mm deflection were calculated. The findings suggest that: 1. Align demonstrated statistically significant increase in loading force (p<0.05) and unloading force (p<0.01) at 3mm deflection after recycling(T2), but NiTi, Optimalloy and Sentalloy showed no statistically difference after recycling. 2. Align demonstrated statistically significant decrease in hysteresis(p<0.01) after recycling(T2) but NiTi, Optimalloy and Sentalloy showed no statistically significant difference after recycling. 3. All wires showed no statistically significant difference in loading force at 1mm deflection after recycling(T2). 4. Align demonstrated statistically significant decrease in unloading force in 1mm deflection (p<0.05) after recycling(T2) but NiTi, Optimalloy and Sentalloy showed no statistically difference after recycling. 5. Loading force and unloading force of T1 showed no significant change compared with those of T0, but loading force and unloading force of T2 showed significant changes compared with those of T0(p<0.05, p<0.01 respectively). 6. Align demonstrated a tendency to lose some of this pseudoelsticity in T1 and pseudoplasticity and pseudoelasticity in T2.
Subject(s)
Alloys , Nickel , Recycling , Saliva, Artificial , TitaniumABSTRACT
The purpose of this study is to investigate the changes of mechanical properties and surface topography of various nickel titanium wires after heat sterilization for recycling with quantitative method. The materials used were four kinds of nickel titanium orthodontic wires including a Korean product. Experimental specimens were treated with two kinds of heat sterilization methods; dry heat (180degrees C, 60snin) and autoclave (121degrees C, 15-20psi, 30min). Mechanical properties were evaluated by tensile test with Instron 4466 (load cell capacity : 1000 kg, cross head speed : 5mm/min, grip distance : 40mm, in room temperature). Surface topography of various wires was compared with each other qualitatively by using scanning electron microscopy and quantitatively by using profilometer. The findings were analyzed statistically with student t-tests. The results were as follows; 1. Neither method of heat sterilization hod any effects on tensile properties of the nickel-titanium wires used in this experiment. 2. Before heat sterilization, the surface smoothness was highest in Optimalloy, followed by Align and Sentailoy, with NiTi showing the lowest smoothness value. 3. In surface topography, Align and Optimalloy were not influenced by heat sterilization. NiTi, on the other hand, had increased roughness after dry heat sterilization and Sentalloy showed the same tendency after each of the two heat sterilization procedures.