Effect of casting atmosphere on the shear bond strength of a ceramic to Ni-Cr and Ni-Cr-Be alloys

The success of metal-ceramic restorations depends on an optimal bond between metal and ceramic. This study evaluated the effect of 3 casting atmospheres on the metal-ceramic bond strength (MCBS) of 2 Ni-Cr alloys, with beryllium (Fit Cast V) and without beryllium (Fit Cast SB). Sixty acrylic resin patterns (8 mm long and 5 mm diameter) were obtained using a fluorocarbon resin matrix. Wax was used to refine the surface of acrylic resin patterns that were invested and cast in an induction casting machine under normal, vacuum, and argon atmospheres at a temperature of 1340ºC. The castings were divested manually and airborne-particle abraded with 100-µm aluminum-oxide. Ten castings were obtained for each group. The IPS Classic V ceramic was applied (2 mm high and 5 mm diameter). The shear bond strength was tested in a mechanical testing machine with a crosshead speed of 2.0 mm/min. The MCBS data (MPa) were subjected to 2-way analysis of variance (α=0.05). There was no statistically significant difference (p>0.05) between the alloys or among the casting atmospheres. Within the limitations of this study, it may be concluded that the presence of beryllium and the casting atmosphere did not interfere in the MCBS of the evaluated metal-ceramic combinations

O sucesso das restaurações metalocerâmicas depende da ótima união entre metal e cerâmica. Este estudo avaliou o efeito de 3 atmosferas de fundição na resistência de união metalocerâmica (RUMC) de 2 ligas de Ni-Cr, com berílio (Fit Cast V) e sem berílio (Fit Cast SB). Sessenta padrões de resina acrílica (comprimento de 8 mm e diâmetro de 5 mm) foram obtidos usando uma matriz de teflon. Foi utilizada cera para refinar a superfície dos padrões de resina acrílica que foram incluídos e fundidos em máquina de fundição por indução nas seguintes atmosferas de fundição: normal, vácuo e argônio, à temperatura de 1340ºC. As fundições foram removidas e usinadas com partículas de óxido de alumínio de 100 mm, sendo 10 fundições por grupo. Foi aplicada a cerâmica IPS Clássico V (2 mm de altura e diâmetro de 5 mm). O ensaio de cisalhamento foi realizado em máquina de ensaios mecânicos com velocidade de 2,0 mm/min. Os dados de RUMC (MPa) foram analisados por meio da análise de variância (α=0,05). Não houve diferença significante (p>0,05) entre as ligas e entre as atmosferas de fundição. Dentro das limitações deste estudo, pode-se concluir que a presença do berílio e a atmosfera de fundição não interferiram na RUMC das combinações metalocerâmicas avaliadas.

Effects of cryogenic treatment on the corrosion resistance of the nickel-chromium alloys / 实用口腔医学杂志

Objective:To investigate the feasibility of improving the corrosion resistance of nickel-chromium alloys by the means of cryogenic treatment. Methods:16 disk samples were divided into 4 groups, including control group(C), cryotreat group(E1),tempering after cryotreat group(E2) and simulative porcelain sintering after cryotreat group(E3). All samples were subjected to electrochemical potentiodynamic polarization after immersed in the artificial saliva ISO/TR 10271:1993(E) pH 6.8 for 24 h at ambient temperature. The metallography of all groups were observed by SEM. Results:①Cryogenic treatment elevated the pitting corrosion potential and dropped the corrosion current of Ni-Cr alloys. Following simulative porcelain sintering,as well as tempering after cryotreat, decreased the corrosion current. But the corrosion potential of Ni-Cr alloys fell after cryotreat and following simulative porcelain sintering. Tempering after cryotreat did not affect the pitting corrosion potential. ②Much small secondary substance separated out and evenly distributed along the crystals of Ni-Cr alloys after cryotreat. Conclusion:Cryogenic treatment effectively improves the electrochemical corrosion resistance of Ni-Cr alloys, and tempering following cryotreat is unnecessary. It is not recommended to sintering porcelain after cryogenic treatment.