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West China Journal of Stomatology ; (6): 642-645, 2015.
Article Dans Chinois | WPRIM | ID: wpr-317747

Résumé

<p><b>OBJECTIVE</b>To evaluate the effect of microwave sintering on the translucency of zirconia and to compare these effect with those of conventional sintering. The relationship between the microstructure of specimens and translucency was investigated.</p><p><b>METHODS</b>A total of 10 disc-shaped specimens were fabricated from 2 commercial brands of zirconia, namely, Zenostar and Lava. Each group included 5 discs. Conventional sintering was performed according to the manufacturers' specifications. The maximum temperature for Zenostar was 1,490 °C, whereas that for Lava was 1,500 °C. The dwelling time was 2 h. The sintering temperature for microwave sintering was 1,420 °C, heating rate was 15 °C · min⁻¹, and dwelling time was 30 min. After sintering, the translucency parameter (TP) of the specimens were measured with ShadeEye NCC. The sintered density of the specimens was determined by Archimedes' method. The grain size and microstructure of the specimens were investigated by scanning electron microscopy.</p><p><b>RESULTS</b>Density and translucency slightly increased by microwave sintering, but no significant difference was found between microwave and conventional sintering (P > 0.05). Small and uniform microstructure were obtained from microwave sintering. The mean TP of Lava was significantly higher than that of Zenostar (P < 0.001).</p><p><b>CONCLUSION</b>The translucency of zirconia sintered by microwave sintering is similar to that of the zirconia sintered by conventional sintering.</p>


Sujets)
Céramiques , Chimie , Conception de prothèse dentaire , Méthodes , Chauffage , Test de matériaux , Microscopie électronique à balayage , Micro-ondes , Propriétés de surface , Technologie dentaire , Méthodes , Zirconium , Chimie
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