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China Journal of Chinese Materia Medica ; (24): 207-211, 2012.
Article Dans Chinois | WPRIM | ID: wpr-288671

Résumé

In this study, products of psoralen pyrolysis were detected using a solid pyrolysis apparatus and synchrotron radiation vacuum ultraviolet photoionization mass spectrum (SVUV-PIMS). The pyrolytic kinetics of psoralen was also studied by calculating its initial pyrolytic route in quantum chemistry. According to the findings with SVUV-PIMS, three pyrolytic products were observed, CO, C9H6O and C10H6O2. Theoretically, three fragment pathways were calculated for psoralen, in which the major primary decomposition route was de-CO, and the major secondary decomposition reaction was de-CO reaction of de-CO products.


Sujets)
Monoxyde de carbone , Chimie , Psoralène , Chimie , Température élevée , Cinétique , Spectrométrie de masse , Méthodes , Modèles chimiques , Structure moléculaire , Composés chimiques organiques , Chimie , Synchrotrons , Rayons ultraviolets , Vide
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