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1.
Acta Pharmaceutica Sinica B ; (6): 564-567, 2016.
Artigo em Inglês | WPRIM | ID: wpr-256794

RESUMO

Two new phenylpropanoid glycosides named cuneataside E () and cuneataside F (), were isolated from the aerial parts of(Dum. Cours.) G. Don, whose structures wereandisomer, respectively. Their structures were elucidated on the basis of comprehensive spectroscopic analysis (UV, IR, HR-ESI-MS, 1D and 2D NMR). Inbioassays at 10 μmol/L, compoundshowed moderate hepatoprotective activity against-acetyl--aminophenol (APAP)-induced toxicity in HeG2 cells.

2.
China Journal of Chinese Materia Medica ; (24): 1028-1031, 2011.
Artigo em Chinês | WPRIM | ID: wpr-252949

RESUMO

In order to study the chemical constituents of the leaves of Tripterygium wilfordii and provide references for the bio-active study, we isolated nine compounds from the dried leaves of Tripterygium wilfordii. Their structures were determined by application of spectroscopic (NMR, MS) and chemical methods. These compounds were isolated and identified as (+)-lyoniresinol (1), (+)-isolariciresinol (2), burselignan (3), dibutyl phthalate (4), cyclo-(S-Pro-R-Phe) (5), cyclo-(S-Pro-R-Leu) (6), cyclo-(S-Pro-S-Ile) (7), 3-hydroxy-1-(4-hydroxy-3,5-dimethoxyphenyl)-1-propanone (8) and daucosterol (9). Compounds 1-3, 5-8 were isolated from this plant for the first time.


Assuntos
Anisóis , Química , Dibutilftalato , Química , Lignina , Química , Imageamento por Ressonância Magnética , Métodos , Espectrometria de Massas , Métodos , Naftalenos , Química , Naftóis , Química , Peptídeos Cíclicos , Química , Extratos Vegetais , Química , Folhas de Planta , Química , Sitosteroides , Química , Tripterygium , Química
3.
China Journal of Chinese Materia Medica ; (24): 714-717, 2010.
Artigo em Chinês | WPRIM | ID: wpr-281732

RESUMO

<p><b>OBJECTIVE</b>To study the chemical constituents of the plant of Sarcandra glabra and provide reference for the study of the bioactive substances.</p><p><b>METHOD</b>The compounds were isolated from the EtOH extract by various chromatographic methods and their structures were elucidated by their physico-chemical properties and the analysis of their spectral data.</p><p><b>RESULT</b>Nine compounds were isolated and identified as isoscopletin (1), syringaresinol monoside (2), styraxjaponoside B (3), 5-O-caffeoylshikimic acid (4), shizukanolide E (5), isoastilbin (6), neoisoastilbin (7), astilbin (8), neoastilbin (9).</p><p><b>CONCLUSION</b>Compounds 1-7 were isolated from S. glabra for the first time.</p>


Assuntos
Colestenonas , Medicamentos de Ervas Chinesas , Química , Flavonoides , Flavonóis , Furanos , Lignanas , Magnoliopsida , Química , Casca de Planta , Química , Caules de Planta , Química , Ácido Chiquímico
4.
China Journal of Chinese Materia Medica ; (24): 997-1000, 2010.
Artigo em Chinês | WPRIM | ID: wpr-281671

RESUMO

<p><b>OBJECTIVE</b>To study the chemical constituents of the leaf of Clausena lansium (Lour.) Skeels.</p><p><b>METHOD</b>The compounds were isolated by various chromatographic techniques and their structures were elucidated by their physicochemical properties and the analysis of their spectroscopic data.</p><p><b>RESULT</b>Seven compounds were isolated and identified as corchoionoside C (1), 1'-O-beta-D-glucopyranosyl (2R,3S)-3-hydroxynodakenetin (2), quercetin-3-O-robinobioside (3), rutin (4), quercetin-3-O-scillabioside (5), keampferol-3-O-alpha-L-rhamnopyranosyl(1-->2) [alpha-L-rhamnopyranosyl(1-->6)]-beta-D-glucopyranoside (6), mauritianin (7).</p><p><b>CONCLUSION</b>Compounds 1-7 were isolated from the genus Clausena for the first time.</p>


Assuntos
Fenômenos Químicos , Cromatografia Líquida de Alta Pressão , Clausena , Química , Compostos Orgânicos , Química
5.
China Journal of Chinese Materia Medica ; (24): 3007-3009, 2010.
Artigo em Chinês | WPRIM | ID: wpr-260699

RESUMO

In order to study the chemical constituents of the plant of Hydrangea paniculata and provide reference for the study of the bioactive substances, we isolated nine compounds from the dried branches of H. paniculata. Their structures were determined by application of spectroscopic (NMR, MS) and chemical methods. These compounds were identified as skimmin (1), isotachioside (2), 8-methoxy-7-O-beta-D-glucopyranosyloxy coumarin glycoside (3), scopolin (4), 1-(alpha-L-rhamnosyl-(1 --> 6) -O-beta-D-glucopyranosyloxy) - 3, 4, 5-trimethoxybenzene (5), apiosylskimmin (6), umbelliferone (7), scopoletin (8), 7-hydroxy-8-methoxycoumarin (9). Compounds 1 - 7 were isolated from H. paniculata for the first time.


Assuntos
Medicamentos de Ervas Chinesas , Hydrangea , Química
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