The comparison of relative reliability on biaxial and three point flexural strength testing methods of light curing composite resin / 대한치과보존학회지

The possibility of applying a bi-axial flexure strength test on composite resin was examined using three point and bi-axial flexure strength tests to measure the strength of the light-cured resin and to compare the relative reliability using the Weibull modulus. The materials used in this study were light-curing restorative materials, MICRONEW(TM), RENEW(R) (Bisco, Schaumburg, USA). The bi-axial flexure strength measurements used the piston-on-3-ball test according to the regulations of the International Organization for Standardization (ISO) 6872 and were divided into 6 groups, where the radius of the specimens were 12 mm (radius connecting the 3-balls: 3.75 mm), 16 mm (radius connecting the 3-balls: 5 mm), and the thickness were 0.5 mm, 1 mm, 2 mm for each radius. The bi-axial flexure strength of the MICRONEW(TM) and RENEW(R) were higher than the three point flexure strength and the Weibull modulus value were also higher in all of the bi-axial flexure strength groups, indicating that the bi-axial strength test is relatively less affected by experimental error. In addition, the 2 mm thick specimens had the highest Weibull modulus values in the bi-axial flexure strength test, and the MICRONEW(TM) group showed no significant statistical difference (p > 0.05). Besides the 2 mm MICRONEW(TM) group, each group showed significant statistical differences (p < 0.05) according to the thickness of the specimen and the radius connecting the 3-balls. The results indicate that for the 2 mm group, the bi-axial flexure strength test is a more reliable testing method than the three point flexure strength test.

Mechanical Properties Of Reused Lithium Disilicate Glass-Ceramic Of Ips Empress 2 System / 대한치과보철학회지

This investigation was designed to estimate the biaxial flexure strength and fracture toughness of lithium disilicate glass-ceramics of IPS Empress 2 system pressed with as-received ingots and their sprue buttons. Two groups of the lithium disilicate glass-ceramics were prepared as follows: group 1 is ingot-pressed group; group 2 is sprue button-pressed group. A ball-on-three-ball test was used to determine biaxial flexure strength (BFS) of disks in wet environment. Scanning electron microscopy(SEM) analysis was conducted to observe the microstructure of the ceramics. Unpaired t-test showed that there were no differences in the mean biaxial flexure strength (BFS) and KIC values between group 1 and 2 (p>0.05). Two groups showed similar values in the KIC and the strength at 5% failure probability. The SEM micrographs of the IPS Empress 2 glass-ceramic showed a closely packed, multi-directionally interlocking pattern of numerous lithium disilicate crystals protruding from the glass matrix. The lithium orthophosphate crystals could not be observed on the fracture surface etched. There was no a marked difference of the microstructure between group 1 and 2. Although there were no tests including color stability, casting accuracy, etc., the results of this study implied that we could reuse the sprue button of the pressed lithium disilicate glass-ceramic of IPS Empress 2 system.

EFFECT OF CeCO2 ADDITION IN GLASS COMPOSITION ON THE STRENGTH OF ALUMINA-GLASS COMPOSITES / 대한치과보철학회지

Dental ceramics have good aesthetics, biocompatibility, low thermal conductivity, abrasion resistance, and color stability. However, poor resistance to fracture and shrinkage during firing process have been limiting factors in their use, particularly in multiunit ceramic restorations. A new method for making all-ceramic crowns that have high strength and low processing shrinkage has been developed and is referred to as the Vita In-Ceram method. This study was performed to investigate the effect of Ce02 addition in borosilicate glasses on the strength of alumina-glass composites. Porous alumina compacts were prepared by slip casting and sintered at 1,100 degrees C for 2 hours. Dense composites were made by infiltration of molten glass into partially sintered alumina at 1,140 C for 4 hours. Specimens were polished sequentially from #800 to #2000 diamond disk, and the final surface finishing on the tensile side was received an additional polishing sequence through 1,cm diamond paste. Biaxial flexure test was conducted by using ball-on-three-ball method at a crosshead speed of 0.5mm/min. To examine the microstructural aspect of crack propagation in the alumina-glass composites, Vickers-produced indentation crack was made on the tensile surface at a load of 98.0 N and dwell time of 15 sec, and the radial crack patterns were examined by an optical microscope and a scanning electron microscope. The results obtained were summarized as follows ; 1. The porosity rates of partially sintered alumina decreased with the rising of firing temperature. 2. The maximum biaxial flexure strength of 423.5MPa. in alumina-glass composites was obtained with an addition of 3 mol% Ce02 in glass composition and strength values showed the aspect of decrease with the increase of Ce02 content. 3. The biaxial flexure strength values of alumina-glass composites were decreased with rising the firing temperature. 4. Observation of the fracture surfaces of alumina-glass composites indicated that the enhancement of strength in alumina-glass composites was due to the frictional or geometrical interlocking of rough fracture surfaces and ligamentary bridging by intact islands of materials left behind the fracture front.