The effects of deproteinization and primer treatment on microtensile bond strength of self-adhesive resin cement to dentin / 대한치과재료학회지

The purpose of this study was to evaluate the effects of deproteinization and an additional primer treatment on the microtensile bond strength of a newly developed self-adhesive resin cement to dentin. The occlusal dentin of extracted human third molars was randomly divided into four groups according to the surface treatment: a control (CON) with no treatment; applying a deproteinizing agent (DPT) (5% sodium hypochlorite); using a primer (PRI) (G-CEM ONE Adhesive enhancing primer, GC); and applying a deproteinizing agent and a primer (DPT-PRI). Composite resin blocks with a disk shape (diameter, 10 mm; height, 4 mm) were bonded to the treated dentin using a self-adhesive resin cement (G-CEM ONE, GC). The specimens were sectioned into sticks with a cross-section of 1 mm² and tested to failure in tension mode at a crosshead speed of 1 mm/min. All groups showed a significantly higher microtensile bond strength compared to CON (p0.05). Within the limitations of this study, a deproteinizing agent or specific primer can enhance the microtensile bond strength of the self-adhesive resin cement to dentin. However, it is not recommended to use a primer in combination with the deproteinizing agents.

Evaluation of shear-bond strength between different self-adhesive resin cements with phosphate monomer and zirconia ceramic before and after thermocycling / 대한치과보철학회지

PURPOSE: This study compared shear bond strengths of five self-adhesive cements with phosphate monomer to zirconium oxide ceramic with and without airborn particle abrasion. MATERIALS AND METHODS: One hundred zirconia samples were air-abraded (50 microm Al2O3). One hundred composite resin cylinders were fabricated. Composite cylinders were bonded to the zirconia samples with either Permacem 2.0 (P), Clearfil(TM) SA Luting (C), Multilink(R) Speed (M), RelyX(TM) U200 Automix (R), G-Cem LinkAce(TM) (G). All bonded specimens were stored in distilled water (37degrees C) for 24 h and half of them were additionally aged by thermocycling (5degrees C, 55degrees C, 5,000 times). The bonded specimens were loaded in shear force until fracture (1 mm/min) by using Universal Testing Machine (Model 4201, Instron Co, Canton, MA, USA). The failure sites were inspected under field-emission scanning electron microscopy. The data was analyzed with ANOVA, Tukey HSD post-hoc test and paired samples t-test (alpha=.05). RESULTS: Before and after thermocycling, Multilink(R) Speed (M) revealed higher shear-bond strength than the other cements. G-Cem LinkAce(TM) (G) showed significantly lower bond strengths after thermocycling than before treatment (P.05). CONCLUSION: Most self-adhesive cements with phosphate monomer showed high shear bond strength with zirconia ceramic and weren't influenced by thermocycling, so they seem to valuable to zirconia ceramic bonding.

Effect of dentin pretreatment and curing mode on the microtensile bond strength of self-adhesive resin cements

PURPOSE: The aim was to evaluate the effect of curing mode and different dentin surface pretreatment on microtensile bond strength (microTBS) of self-adhesive resin cements. MATERIALS AND METHODS: Thirty-six extracted human permanent molars were sectioned horizontally exposing flat dentin surface. The teeth were divided into 12 groups (3 teeth/group) according to the dentin surface pretreatment methods (control, 18% EDTA, 10% Polyacrylic acid) and curing mode (self-curing vs. light-curing) of cement. After pretreatment, composite resin blocks were cemented with the following: (a) G-CEM LinkAce; (b) RelyX U200, followed by either self-curing or light-curing. After storage, the teeth were sectioned and microTBS test was performed using a microtensile testing machine. The data was statistically analyzed using one-way ANOVA, Student T-test and Scheffe's post-hoc test at P<.05 level. RESULTS: For G-CEM LinkAce cement groups, polyacrylic acid pretreatment showed the highest microTBS in the self-cured group. In the light-cured group, no significant improvements were observed according to the dentin surface pretreatment. There were no significant differences between curing modes. Both dentin surface pretreatment methods helped to increase the microTBS of RelyX U200 resin cement significantly and degree of pretreatment effect was similar. No significant differences were found regarding curing modes except control groups. In the comparisons of two self-adhesive resin cements, all groups within the same pretreatment and curing mode were significantly different excluding self-cured control groups. CONCLUSION: Selecting RelyX U200 used in this study and application of dentin surface pretreatment with EDTA and polyacrylic acid might be recommended to enhance the bond strength of cement to dentin.

Shear bond strength of three self-adhesive resin cements to dentin.

Context: The result of the studies concerning the bonding of self-adhesive resin cements to dentin is controversial. Aims: To assess in vitro shear bond strength (SBS) of three self-adhesive dual-cured resin cements to dentin compared to a currently used dual-cured resin cement, using SBS test. Settings and Design: The extant study is an experimental in vitro one on extracted human third molars dentin. Material and Methods: 40 intact human third molars were selected and randomly divided into 4 groups of 10. Buccal dentin surfaces were exposed perpendicular to the long axis and prepared with SiC papers. A translucent plastic ring, was placed over the dentin surfaces. Group I (Control group): After 15 s of etching and application of Excite DSC Bond (Ex), Variolink II (Var II) resin cement was injected into the plastic ring and was light cured for 40 s. Group II: RelyX Unicem (RX) was injected into the plastic ring and after 30 s, was light cured for 40 s. Group III: Maxcem (Mc) was injected into the plastic ring and after 30 s, was light cured for 40 s. Group IV: Multilink Sprint (MS) was injected into the plastic ring and after 30 s, was light cured for 40 s. After thermal cycling, SBS were measured with a universal testing machine. Statistical Analysis Used: Statistical computations were conducted according to Student's t-test. Results: The mean SBS and standard deviations (in parentheses) for groups I, II, III, and IV were 12.95 (2.64), 6.73 (0.79), 3.01 (0.90), 4.60 (0.75) MPa, respectively. Statistical analysis, revealed that: (1) the mean SBS of Var II were significantly higher than the other groups (P<0.05). (2) The mean SBS of Mc and MS were significantly lower than RX (P<0.05). (3) The mean SBS of Mc and MS did not show significant difference (P>0.05). Conclusion: Bond strength of three self-adhesive resin cements was significantly lower than the conventional total-etch resin cement. RX significantly performed better SBS than Mc and MS to dentin.

Effect of dentin surface wetness on tensile bond strength of self adhesive resin cements / 대한치과보존학회지

The purpose of this study was to compare the tensile bond strength of several self-adhesive resin cements bonded to dentin surfaces with different wet conditions. Three self-adhesive resin cements; Rely-X Unicem (3M ESPE, St. Paul, MN, USA), Embrace Wetbond (Pulpdent, Oakland, MA, USA), Maxcem (Kerr, Orange, CA, USA) were used. Extracted sixty human molars were used. Each self-adhesive resin cement was adhered to the dentin specimens (two rectangular sticks from each molar) in different wet conditions. Tensile bond strength were measured using universal testing machine (EZ Test, Shimadzu corporation, Kyoto, Japan) at a crosshead speed of 1.0mm/min. After the testing, bonding failures of specimens were observed by Operative microscope (OPMI pro, Carl Zeiss, Oberkochen, Germany). T-test was used to evaluate the effect of dentin surface wetness. One-way ANOVA test was used to evaluate the tensile bond strength of self-adhesive resin cements in the same condition. Scheffe's test was used for statistical analyzing at the 95% level of confidence. The result showed that wetness of dentin surface didn't affect tensile bond strength of self-adhesive resin cements and Maxcem showed the lowest tensile bond strength.