Determination of synephrine and N-methyltyramine in Pericarpium Citri Reticulatae viride by HPLC / 中国中药杂志
China Journal of Chinese Materia Medica
;
(24): 537-539, 2004.
Article
in Chinese
| WPRIM
| ID: wpr-256313
ABSTRACT
<p><b>OBJECTIVE</b>To establish a quantitative method for determination of synephrine and N-methyltyramine in Citri Reticulatae.</p><p><b>METHOD</b>Samples were extracted with 30% methanol. ODS column was used with methanol-water-sodium dodecyl sulfate (55450.1) as mobile phase. Detection wavelength was 285 nm.</p><p><b>RESULT</b>Synephrine and N-methyltyramine in sample solution were well separated. Linearity of synephrine was good (r = 0.9999) in range of 0.35-11.24 microg. The average recovery was 97.1%, and RSD of repeatability was 1.9%.</p><p><b>CONCLUSION</b>This method can be used for quality control of Citri Reticulatae.</p>
Full text:
Available
Index:
WPRIM (Western Pacific)
Main subject:
Plants, Medicinal
/
Quality Control
/
Seasons
/
Synephrine
/
Tyramine
/
Chemistry
/
Chromatography, High Pressure Liquid
/
Citrus
/
Fruit
Language:
Chinese
Journal:
China Journal of Chinese Materia Medica
Year:
2004
Type:
Article
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