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Determination of triterpenoic acids in fruits of Ziziphus jujuba using HPLC-MS with polymeric ODS column / 中国中药杂志
China Journal of Chinese Materia Medica ; (24): 848-851, 2013.
Article in Chinese | WPRIM | ID: wpr-318631
ABSTRACT
A simple and sensitive method has been developed to simultaneously determine betunilic acid, oleanolic acid and ursolic acid in the fruits of Ziziphus jujuba from different regions by HPLC-MS. This HPLC assay was performed on PAH polymeric C18 bonded stationary phase column with mobile phase contained acetonitrile-water (90 10) and with negative ESI detection mode. The developed approach was characterized by short time consumption for chromatographic separation, high sensitivity and good reliability so as to meet the requirements for rapid analysis of large-batch fruits of Z. jujuba from different habitats.
Subject(s)
Full text: Available Index: WPRIM (Western Pacific) Main subject: Polymers / Mass Spectrometry / Triterpenes / Chemistry / Chromatography, High Pressure Liquid / Ziziphus / Fruit / Methods Language: Chinese Journal: China Journal of Chinese Materia Medica Year: 2013 Type: Article

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Full text: Available Index: WPRIM (Western Pacific) Main subject: Polymers / Mass Spectrometry / Triterpenes / Chemistry / Chromatography, High Pressure Liquid / Ziziphus / Fruit / Methods Language: Chinese Journal: China Journal of Chinese Materia Medica Year: 2013 Type: Article