Determination of hydrogen selenide in workplace air with atomic fluorescence / 中华劳动卫生职业病杂志
Chinese Journal of Industrial Hygiene and Occupational Diseases
;
(12): 144-145, 2012.
Article
in Chinese
| WPRIM
| ID: wpr-324243
ABSTRACT
<p><b>OBJECTIVE</b>To determined hydrogen selenide in workplace air with atomic fluorescence.</p><p><b>METHOD</b>Hydrogen selenide were sampled with 0.1 mol/L sodium hydroxide solution in multi-hole absorbing tubes. The sampled absorbing solution were digested with (9+1) nitric acid/perchloric acid. The selenide in sample were reduced by potassium borohydride in 5.0% hydrochloride solution and determined with atomic fluorescence.</p><p><b>RESULTS</b>There was a good linearity (r=0.9999) over the concentration of 0-150 microg/L, The precision of low, middle and high concentration were 3.1%, 7.4% and 6.7%, respectively. The sample collection rate can reach 99%.</p><p><b>CONCLUSION</b>The method was accurate and sensitive to detect hydrogen selenide in workplace air.</p>
Full text:
Available
Index:
WPRIM (Western Pacific)
Main subject:
Spectrometry, Fluorescence
/
Spectrophotometry, Atomic
/
Workplace
/
Selenium Compounds
/
Air Pollutants, Occupational
Language:
Chinese
Journal:
Chinese Journal of Industrial Hygiene and Occupational Diseases
Year:
2012
Type:
Article
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