Determination of fraxinellone in root bark of Dictamnus dasycarpus by RP-HPLC / 中国中药杂志
China Journal of Chinese Materia Medica
; (24): 992-994, 2006.
Article
in Zh
| WPRIM
| ID: wpr-351802
Responsible library:
WPRO
ABSTRACT
<p><b>OBJECTIVE</b>To develop a RP-HPLC method for determination of fraxinellone in Dictamnus dasycarpus.</p><p><b>METHOD</b>RP-HPLC conditions were as follows: AT-LICHROM C18(4.6 mm x 250 mm) column, MeOH-H2O (70:30) as a mobile phase, detection wavelength 240 nm, column temperature 25 degrees C, Flow velocity 0.5 mL x min(-1).</p><p><b>RESULT</b>Linear relationship is very good (r = 0.9999) in 0.018-0.18 mg x mL(-1). The average recovery is 98.9%, RSD is 1.2% (n = 4).</p><p><b>CONCLUSION</b>The method is simple and repeatable and can be used for quantitative analysis of fraxinellone in root bark of D. dasycarpus.</p>
Full text:
1
Index:
WPRIM
Main subject:
Plants, Medicinal
/
Quality Control
/
Benzofurans
/
Chemistry
/
Reproducibility of Results
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Chromatography, High Pressure Liquid
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Plant Roots
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Dictamnus
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Methods
Language:
Zh
Journal:
China Journal of Chinese Materia Medica
Year:
2006
Type:
Article