Determination of cholesteryl palmitate in Oviductus Ranae by HPLC / 中国中药杂志
China Journal of Chinese Materia Medica
;
(24): 990-991, 2005.
Article
in Chinese
| WPRIM
| ID: wpr-358043
ABSTRACT
<p><b>OBJECTIVE</b>To develop a new method for the determination of cholesteryl palmitate in Oviductus Ranae.</p><p><b>METHOD</b>A HPLC method was set up, using Zorbax Silica column and cyclohexane-diethyl ether (401) as mobile phase with a flow rate of 1.0 mL x min(-1), and the UV detection wavelength was 203 nm.</p><p><b>RESULT</b>The calibration curve was linear over the range of 0.60-8.92 microg (r = 0.9997), the average recovery of the method was 98.4%. RSD 1.8% (n = 6).</p><p><b>CONCLUSION</b>The results showed that method was reliable and accurate.</p>
Full text:
Available
Index:
WPRIM (Western Pacific)
Main subject:
Oviducts
/
Quality Control
/
Rana temporaria
/
Materia Medica
/
Chemistry
/
Cholesterol Esters
/
Chromatography, High Pressure Liquid
/
Methods
Limits:
Animals
Language:
Chinese
Journal:
China Journal of Chinese Materia Medica
Year:
2005
Type:
Article
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