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Determination of Nuezhenide and Apigenin 7-O-neohesperidoside in Shanxiangyuan tablets by HPLC / 国际中医中药杂志
International Journal of Traditional Chinese Medicine ; (6): 519-521, 2012.
Article in Chinese | WPRIM | ID: wpr-418829
ABSTRACT
ObjectiveTo establish a method for the determination of Nuezhenide and Apiganin 7-O-neohesperidoside in Shanxiangyuan tablets.Methods The Luna C1s column was used,the mobile phase consisted of HCN-0.5%H3PO4(41 ∶ 59),the flow rate was 1.0 ml/min,the column temperature was 30℃,the UV detector was set at 336nm.Results The linear response range was 0.016~0.32 mg/ml (r=0.9997) and 0.006~0.11 mg/ml respectively.The average recovery rate was 99.0% and 97.5% respectively,RSD was 1.83% and 1.57% respectively,ConclusionThe method was simple,accurate and repeatable.It can be applied in quantitative determination of Nuezhenide and Apigenin 7-O-neohesperidoside in Shanxiangyuan tablets.

Full text: Available Index: WPRIM (Western Pacific) Language: Chinese Journal: International Journal of Traditional Chinese Medicine Year: 2012 Type: Article

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Full text: Available Index: WPRIM (Western Pacific) Language: Chinese Journal: International Journal of Traditional Chinese Medicine Year: 2012 Type: Article