Determination of Schaftoside in Jinshaniu Huashi Tablets by HPLC / 中国药师
China Pharmacist
;
(12): 1224-1225, 2016.
Article
in Chinese
| WPRIM
| ID: wpr-494897
ABSTRACT
Objective:
To establish an HPLC method to determine the content of schaftoside in Jinshaniu Huashi tablets .Meth-odsThe separation was performed on an Agilent ZORBAX SB-C18 column(150 mm ×4.6 mm, 5 μm)with 0.2% phosphoric acid-acetonitrile as the mobile phase with gradient elution at a flow rate of 1.0 ml· min-1 .The detection wavelength was set at 272 nm, and the column temperature was set at 25 ℃.Results:
The calibration curve of schaftoside had a good linearity within the range of 4.58-183.15 μg· ml-1(r=1.000 0).The average recovery was 99.65%with RSD of 1.09%(n=6).Conclusion:
The established method is simple and accurate with high repeatability , which can be used for the content determination of schaftoside in Jinshaniu Hua-shi tablets .
Full text:
Available
Index:
WPRIM (Western Pacific)
Language:
Chinese
Journal:
China Pharmacist
Year:
2016
Type:
Article
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