Study on the Quality Standard for Fufang Ningshen Granule / 中国药房
China Pharmacy
;
(12): 4285-4287, 2016.
Article
in Chinese
| WPRIM
| ID: wpr-503386
ABSTRACT
OBJECTIVE:
To establish the quality standards for Fufang ningshen granule.METHODS:
TLC was used for the qualitative identification of Radix angelicae and White paenoy;HPLC was adopted for the contents determination of spinosin and verbascosidethe column was Kromasil C18 with the mobile phase of acetonitrile-0.1% acetic acid(16∶84,V/V)at a flow rate of 1.0 ml/min,detection wavelength was 330 nm,column temerpature was 30 ℃.RESULTS:
The TLC spots of R. angelicae and W. pae-noy were clear with good separation,negative control without interference. The linear range was 0.055 44-0.277 2μg for spinosin(r=0.999 4)and 0.055 98-0.279 9 μg for verbascoside(r=0.999 5);RSDs of precision,stability and reproducibility tests were lower than 3.0%;recoveries were 95.62%-100.53%(RSD=1.77%,n=9) and 95.63%-102.57%(RSD=2.74%,n=9). CONCLU-SIONSThe standard can be used for the quality control of Fufang ningshen granule.
Full text:
Available
Index:
WPRIM (Western Pacific)
Type of study:
Qualitative research
Language:
Chinese
Journal:
China Pharmacy
Year:
2016
Type:
Article
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