Determination of Emodin in Compound Shouwu Mixture by RP - HPLC / 中国药房
China Pharmacy
;
(12)2001.
Article
in Chinese
| WPRIM
| ID: wpr-532198
ABSTRACT
OBJECTIVE:
To establish a RP-HPLC method for the determination of the content of emodin in Compound shouwu mixture.METHODS:
The determination was performed on Diamonsil C_(18) column(150 mm?4.6 mm,5?m) with the mobile phase consisted of methanol- 0.1%phosphoric acid(6832).The detective wavelength was set at 220 nm.RESULTS:
The linear range of emodin was 7.8~78.0?g?mL~(-1)(r= 0.999 8) with an average recovery rate of 98.25%(RSD = 1.09%,n=9).CONCLUSION:
The method is accurate,sensitive and reproducible,and it is applicable for the quality control of the Compound shouwu mixture.
Full text:
Available
Index:
WPRIM (Western Pacific)
Language:
Chinese
Journal:
China Pharmacy
Year:
2001
Type:
Article
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