Determination of the content of sinapine thiocyanate in Qingrehuashiyangyin granules by HPLC / 中华中医药杂志
China Journal of Traditional Chinese Medicine and Pharmacy
;
(12)2006.
Article
in Chinese
| WPRIM
| ID: wpr-566223
ABSTRACT
Objective:
To establish the quality standard of sinapine thiocyanate in Qingrehuashiyangyin granules by HPLC.Methods:
HPLC was performed on Phenomenex C18 Column(250mm?4.6mm,5?m) with acetonitrile-0.08mol/L KH2PO4(1585) as mobile phase.Flow rate was 1.0ml/min and detecting wave length was 326nm.Column temperature at 30℃.Results:
The good linear relationship was obtained in the range of 0.3976--1.988?g(r=0.9998),and the average recovery was 99.0%.Conclusion:
This method is simple,fast and accurate for the quality control of Qingrehuashiyangyin granules.
Full text:
Available
Index:
WPRIM (Western Pacific)
Language:
Chinese
Journal:
China Journal of Traditional Chinese Medicine and Pharmacy
Year:
2006
Type:
Article
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