Determination of prim-o-glucasylcimifugin and 5-o-methylvisammiosode in Yinhua Ganmao Granules by HPLC / 中成药
Chinese Traditional Patent Medicine
;
(12)1992.
Article
in Chinese
| WPRIM
| ID: wpr-574610
ABSTRACT
AIM:
To establish a HPLC method of determining prim-o-glucasylcimifugin and 5-o-methyl-visammiosode in Yinhua Ganmao Granules (Flos Lonicerae Japonicae, Radix Saposhnikovial, Fructus Forsythiae, etc.).METHODS:
A Kromasil C_(18) column was used. The mobile phase was MeOH-Acetonitrile-H_2O(30∶15∶80). The detection wavelength was 254 nm.RESULTS:
The linear range of prim-o-glucasylcimifugin was within 0.157 5-3.780 5 ?g(r=0.999 9), The linear range of 5-o-methylvisammiosode was within 0.164 4-3.945 6 ?g(r=0.999 8). The average recoveries(n=6) were 99.40% and 96.79%, respectively. RSD were 0.6% and 0.8% respectively.CONCLUSION:
The method is simple, reliable, accurate and can be applied to the quality control of the preparation.
Full text:
Available
Index:
WPRIM (Western Pacific)
Language:
Chinese
Journal:
Chinese Traditional Patent Medicine
Year:
1992
Type:
Article
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