HPLC determination of arecoline in Arecae Pericarpium from different habitats / 中国药学杂志
Chinese Pharmaceutical Journal
;
(24): 909-911, 2013.
Article
in Chinese
| WPRIM
| ID: wpr-860370
ABSTRACT
OBJECTIVE:
To establish a quantitative determination method for arecoline in Arecae Pericarpium.METHODS:
The determination was performed on thermo-biobasic SCX column (4.6 mm×250 mm, 5 μm) with mobile phase consisting of acetonitrile-phosphoric acid solution (55;45). The flow rate was 1.0 mL·min-1, the column temperature was 30°C, and the detection wavelength was 215 nm.RESULTS:
The method had good linear relationship for arecoline hydrobromide in the range of 5.2-83.2 μg·mL-1 (r=0.9991). The average recovery (n=9) was 98.8% for arecoline hydrobromide.CONCLUSION:
The method is simple, accurate and specific. It provides a reliable way for evaluating the quality of Arecae Pericarpium.
Full text:
Available
Index:
WPRIM (Western Pacific)
Language:
Chinese
Journal:
Chinese Pharmaceutical Journal
Year:
2013
Type:
Article
Similar
MEDLINE
...
LILACS
LIS