Detection of chloroprene in human blood by headspace gas chromatography / 中国职业医学
China Occupational Medicine
;
(6): 722-727, 2016.
Article
in Chinese
| WPRIM
| ID: wpr-877017
ABSTRACT
OBJECTIVE:
To establish a detection method for chloroprene in human blood by headspace gas chromatography.METHODS:
The blood sample was placed directly in the headspace bottle,after the head space automatic sampling,the target object was detected by gas chromatography with electron capture detector,quantified by external standard method.RESULTS:
The good linearity range of chloroprene was 0. 00-160. 00 μg / L,and the correlation coefficient was 0. 999 4. The detection limit was 0. 10 μg / L and the minimum detectable concentration in blood samples was 0. 10 μg / L. The with-run relative standard deviation( RSD) was 1. 38%-1. 91%,and the between-run RSD was 2. 11%-3. 08%. The average recovery rate was 89. 00%-93. 88%.CONCLUSION:
The method has the features of high sensitivity,wide linear range and simple sample processing,which was suitable for efficient detection for large quantity of samples.
Full text:
Available
Index:
WPRIM (Western Pacific)
Type of study:
Diagnostic study
Language:
Chinese
Journal:
China Occupational Medicine
Year:
2016
Type:
Article
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