Determination of synephrine and arecoline contents in Xiao'er Xiaoji Zhike oral liquid / 中国中药杂志
China Journal of Chinese Materia Medica
;
(24): 1298-1300, 2011.
Artículo
en Chino
| WPRIM
| ID: wpr-252922
ABSTRACT
<p><b>OBJECTIVE</b>To develop a HPLC method for the determination of synephrine and arecoline contents in Xiao'er Xiaoji Zhike oral liquid.</p><p><b>METHOD</b>The analysis was performed on a Symmetry C18 column (4.6 mm x 250 mm, 5 microm) eluted with acetonitrile-methanol-0.1% acetic acid solution (containing potassium dihydrogen phosphate 0.6 g and SDS 1.0 g per 1 000 mL) (15 30 55) as mobile phase. The detection wavelength was set at 215 nm.</p><p><b>RESULT</b>The synephrine and arecoline concentrations had good linear relationship between 0.281 5-2.815 and 0.040 16-0.401 6 microg (r > 0.999 7), and the average recoveries of the two compounds were 97.1% (RSD 1.4%) and 100% (RSD 1.3%), respectively.</p><p><b>CONCLUSION</b>The method is simple, accurate and sensitive.</p>
Texto completo:
Disponible
Índice:
WPRIM (Pacífico Occidental)
Asunto principal:
Arecolina
/
Medicamentos Herbarios Chinos
/
Sinefrina
/
Cromatografía Líquida de Alta Presión
/
Métodos
Idioma:
Chino
Revista:
China Journal of Chinese Materia Medica
Año:
2011
Tipo del documento:
Artículo
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