Content Determination of Berberine Hydrochloride in Fufang Huangge Jiangtang Tablet by UPLC / 中国药房
China Pharmacy
;
(12): 3004-3005, 2016.
Artículo
en Chino
| WPRIM
| ID: wpr-504706
ABSTRACT
OBJECTIVE:
To establish a method for the content determination of berberine hydrochloride in Fufang huangge ji-angtang tablet.METHODS:
UPLC was performed on the column of Acquity UPLC BEH C18 with mobile phase of acetoni-trile-0.1% H3PO4(21∶79,V/V)at flow rate of 0.3 ml/min,the detection wavelength was 345 nm,column temperature was 30℃, and the volume injection was 1.0 μl.RESULTS:
The linear range of berberine hydrochloride was 0.008 16-0.081 6 μg(r=0.999 9);RSDs of precision,stability and reproducibility were lower than 1%;average recovery was 97.05%-98.96%(RSD=0.66%,n=6).CONCLUSIONS:
The method is simple,precise,stablity and reproducible,and can be used for the quality control of Fufang huangge jiangtang tablet.
Texto completo:
Disponible
Índice:
WPRIM (Pacífico Occidental)
Idioma:
Chino
Revista:
China Pharmacy
Año:
2016
Tipo del documento:
Artículo
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