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Quantitative Determination of Ferulic Acid Content in Chrysanthemum Morifolium cv. ( Chuju) Continuous Cropping Soil Using Near Infrared Spectroscopy / 分析化学
Article en Zh | WPRIM | ID: wpr-514431
Biblioteca responsable: WPRO
ABSTRACT
A near infrared spectroscopy ( NIRS) method was used for rapid quality evaluation of ferulic acid content in chrysanthemum morifolium cv. ( Chuju) continuous cropping soil. Standard leverage, studentized residual and Mahalanobis distance were calculated to eliminate abnormal samples. After the initial near infrared spectrum was treated by two second derivative and Norris smoothing filter noise, 6000-4000 cm-1 wave number range and 7 factors were chosen for partial least squares ( PLS) calibration model. The results showed that good correlation was presented between the calibration set/validation set and the values determined by high performance liquid chromatography, and the calibration correlation coefficient ( Rc ) and validation correlation coefficient ( Rcv ) were 0. 9914 and 0. 9935, respectively. Root mean square error of calibration (RMSEC), root mean square error of validation (RMSEP) and root mean square error of cross-validation (RMSECV) were 0. 484, 0. 539 and 0. 615, respectively. This method was accurate, reliable, simple, rapid and nondestructive, and could be applied to the fast analysis for ferulic acid in continuous cropping soil.
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Texto completo: 1 Índice: WPRIM Idioma: Zh Revista: Chinese Journal of Analytical Chemistry Año: 2017 Tipo del documento: Article
Texto completo: 1 Índice: WPRIM Idioma: Zh Revista: Chinese Journal of Analytical Chemistry Año: 2017 Tipo del documento: Article