Determination of 4′-O-?-D-glycosyl-5-O-methylvisamminol in Jingfuzhiyang Granules by RP HPLC / 中成药
Chinese Traditional Patent Medicine
;
(12)1992.
Artículo
en Chino
| WPRIM
| ID: wpr-682534
ABSTRACT
AIM:
To establish a RP HPLC method for the determination of 4′ O ? D glycosyl 5 O methylvisamminol in Jingfuzhiyang Granules (Herba Schizonepetae, Fructus kochiae, Radix Saposhnikoviae, Fructus Crataegi, etc.).METHODS:
The sample was separated on Turnner Kromasil C 18 column (4.6mm?200mm,5?m) with mobile phase of methanol 0.05mol?L -1 potassium dihydrogen phosphate acetic acid isopropyl alcohol (85∶170∶4∶4,v/v). The detection wavelength was set at 254nm and the flow rate was 1.0mL?min -1 . The column temperature was 30℃.RESULTS:
The calibration curve was linear in the range of 0.0606~0.606?g (r=0.9994). The average recovery was 92.2%.CONCLUSION:
This method proves to be relatively simple and accurate, and available for the quality control of Jingfuzhiyang Granules
Texto completo:
Disponible
Índice:
WPRIM (Pacífico Occidental)
Idioma:
Chino
Revista:
Chinese Traditional Patent Medicine
Año:
1992
Tipo del documento:
Artículo
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