Synthesis with spectral investigation of new ligand derived from pyrimidine with some metal complexes / 国际药学研究杂志

ABSTRACT

New ligand were synthesized by two steps in first steps were prepared chalcones compound from reacting of various carbonyl compounds (3-amino acetophenone with salicyldehyde,the second steps were closure of the ring by reacting(chalcones compound(AS) with thiouria, then reaction mixture was reflux for (8h) to produce Pyrimidine derivatives(AST) also prepared some complexes with Fe(II),Co(II), Ni(II),Cu(II),the ligand (AST)with its complexes were characterized by ((FT.IR, Uv-Vis, HNMR, Mass)–spectra,elemental analysis, melting point, molar conductivity).