HPLC Simultaneous Determination of Sodium Danshensu, Hesperidin and Salvianolic ;Acid B in Niaosaitong Capsules / 中国中医药信息杂志
Chinese Journal of Information on Traditional Chinese Medicine
;
(12): 83-85, 2014.
Article
Dans Chinois
| WPRIM
| ID: wpr-446367
ABSTRACT
Objectives To establish an HPLC method for determination of sodium Danshensu, hesperidin and salvianolic acid B in Niaosaitong capsules. Methods Three components were separated by C18 chromatographic column with a gradient mobile phase consisting of acetonitrile and 0.1%phosphoric acid solution at a flow rate of 1.0 mL/min, column temperature of 30 ℃, and detection wavelength was set at 286 nm. Results Sodium Danshensu, hesperidin and salvianolic acid B had good linearity in the range of 0.038 44-1.922 μg, 0.000 207 052 8-4.044 μg, 0.034 28-1.714 μg respectively, and the average recovery rate was 90.9%-107.1%, RSD was 2.1%-3.2%. Conclusion The methods is simple and accurate, and can be used for the quality control of Niaosaitong capsules.
Texte intégral:
Disponible
Indice:
WPRIM (Pacifique occidental)
langue:
Chinois
Texte intégral:
Chinese Journal of Information on Traditional Chinese Medicine
Année:
2014
Type:
Article
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