Study on Quality Standard of Jianpi Fugan Pills / 中国中医药信息杂志
Chinese Journal of Information on Traditional Chinese Medicine
; (12): 47-48,49, 2013.
Article
Dans Zh
| WPRIM
| ID: wpr-598705
Responsable en Bibliothèque :
WPRO
ABSTRACT
Objective To establish the quality standard for Jianpi Fugan Pills. Methods Angelicae Sinenis Radix and Atractylodis Macrocephalae Rhizome in the formulation were qualitatively identified by TLC. The content of ferulic acid was analyzed by HPLC. TIANHE C18 column (250 mm×4.6 mm, 5 μm) was used with a mobile phase of acetonitrile-0.085% phosphorous acid (17∶83). The content was detected at wavelength of 323 nm. The flow rate was 1.0 mL/min, and temperature was 25 ℃. Results The spots in the TLC of Angelicae Sinenis Radix and Atractylodis Macrocephalae Rhizome were in the same chormatograms of control articles. The linear range of ferulic acid was 0.114-1.482 μg. The average recovery was 98.36%and RSD was 1.16%. Conclusion The method is simple, accurate and highly sensitive, which can be used for quality control of Jianpi Fugan Pills.
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Indice:
WPRIM
langue:
Zh
Texte intégral:
Chinese Journal of Information on Traditional Chinese Medicine
Année:
2013
Type:
Article