Experimental Research on the Detection Methods for Toddalolactone in Jinji Tablets / 中国药师
China Pharmacist
;
(12): 2077-2079, 2017.
Article
Dans Chinois
| WPRIM
| ID: wpr-705431
ABSTRACT
Objective:
To identify toddalolactone and establish the analysis method for Jinji tablets.Methods:
An Hypersil DBS C18column(250 mm×4.6 mm,5 μm) was used. The mobile phase consisted of acetonitrile-0.1% phosphoric acid solution. The flow rate was 0.8 ml·min-1and the detection wavelength was at 330 nm. Toddalolactone was identified by an LC-MS method and the re-sult was compared with that of the reference regent.TLC and HPLC analytical methods were used for analysis of toddalolactone.Re-sultsTotally 58 batches of Jinji tablets were tested,and the suspected samples were confirmed by HPLC-MS/MS.Toddalolactone was detected out from 20 batches of samples.Conclusion:
The method is simple,rapid and accurate, which is able to detect toddalolac-tone quickly and effectively.
Texte intégral:
Disponible
Indice:
WPRIM (Pacifique occidental)
Type d'étude:
Etude diagnostique
langue:
Chinois
Texte intégral:
China Pharmacist
Année:
2017
Type:
Article
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