Rapid determination of puerarin in Xiaoke pill powder by near-infrared spectroscopy / 中国中药杂志
China Journal of Chinese Materia Medica
;
(24): 672-675, 2011.
Artigo
em Chinês
| WPRIM
| ID: wpr-247412
ABSTRACT
<p><b>OBJECTIVE</b>To determine the content of puerarin in Xiaoke pill powder rapidly by near-infrared spectroscopy.</p><p><b>METHOD</b>Near-infrared diffuse reflectance spectroscopy technology was used to collect NIR spectra of Xiaoke pills powder. With HPLC analysis values as reference, the fast determination method of puerarin was established with partial least squares (PLS).</p><p><b>RESULT</b>The R2, RMSECV and RPD of the calibration model for puerarin were 0.980 1, 0.131 and 7.09. The average relative deviation of the predication set was 3.2%.</p><p><b>CONCLUSION</b>The method is accurate, fast and simple, which could be generalized to the on-line quality control of Xiaoke pill powder production.</p>
Texto completo:
DisponíveL
Índice:
WPRIM (Pacífico Ocidental)
Assunto principal:
Pós
/
Fatores de Tempo
/
Medicamentos de Ervas Chinesas
/
Espectroscopia de Luz Próxima ao Infravermelho
/
Isoflavonas
/
Métodos
Tipo de estudo:
Estudo prognóstico
Idioma:
Chinês
Revista:
China Journal of Chinese Materia Medica
Ano de publicação:
2011
Tipo de documento:
Artigo
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