Content comparison of buddleoside and pectolinarin in Cirsium japonicum, C. leo and C. leducei / 中国中药杂志
China Journal of Chinese Materia Medica
;
(24): 674-677, 2013.
Artigo
em Chinês
| WPRIM
| ID: wpr-350708
ABSTRACT
<p><b>OBJECTIVE</b>To compare Cirsium japonicum characteristics with C. leo and C. leducei, along with the content of buddleoside and pectolinarin, and lay the foundation for the quality control of C. japonicum.</p><p><b>METHOD</b>Samples were collected and the relevant drugs were bought. The samples were divided into root, stem, leaf and flower, and the content of buddleoside and pectolinarin was determine by the HPLC. Chromatographic column Waters XBridge C18 (4.6 mm x 250 mm), mobile phase methanol-water (45 55), measurement wavelength 326 nm, flow rate 0.8 mL x min(-1), column temperature 30 degrees C. RESULT AND CONDUSION Standard curve equation of buddleoside Y = 74 064X-47 748, R2 = 0.991. Standard curve equation of pectolinarin Y = 1 711 64X - 180 707, R2 = 0.999. The content of buddleoside C. japonicum leaf was 1.987 3%, C. leo leaf 1.412 2%, C. leducei leaf 0.149 2%. The content of buddleoside was lower in root and stem. Pectolinarin was not detected in the C. japonicum and C. leo. The pectolinarin content was 0.069 0% in C. leducei leaf.</p>
Texto completo:
DisponíveL
Índice:
WPRIM (Pacífico Ocidental)
Assunto principal:
Solubilidade
/
Especificidade da Espécie
/
Medicamentos de Ervas Chinesas
/
Química
/
Reprodutibilidade dos Testes
/
Cromatografia Líquida de Alta Pressão
/
Cromonas
/
Cirsium
Idioma:
Chinês
Revista:
China Journal of Chinese Materia Medica
Ano de publicação:
2013
Tipo de documento:
Artigo
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