Application of nuclear magnetic resonance to the determination of the configuration of glycoside bond / 药学学报
Acta Pharmaceutica Sinica
;
(12): 127-131, 2011.
Artigo
em Chinês
| WPRIM
| ID: wpr-353317
ABSTRACT
In the structural determination of natural glycosides, nuclear magnetic resonance (NMR) is an important approach in determining the configuration of glycoside bond. The test of coupling constant of the anomeric proton and chemical shift of the anomeric carbon are two common methods, but these methods are not suitable for some sugars. For those sugars, detailed 13C NMR analysis is an alternative choice. This paper summarizes the characteristics of 1H and 13C NMR data of the common monosaccharides published in the literatures, in order to search an approach to determine the configuration of glycoside bond.
Texto completo:
DisponíveL
Índice:
WPRIM (Pacífico Ocidental)
Assunto principal:
Configuração de Carboidratos
/
Isótopos de Carbono
/
Espectroscopia de Ressonância Magnética
/
Química
/
Glicosídeos
/
Métodos
/
Monossacarídeos
Idioma:
Chinês
Revista:
Acta Pharmaceutica Sinica
Ano de publicação:
2011
Tipo de documento:
Artigo
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