TLC identification and determination of deoxyandrographolide of Compound Kumuxiaoyan Tablets / 中成药
Chinese Traditional Patent Medicine
;
(12)1992.
Artigo
em Chinês
| WPRIM
| ID: wpr-682562
ABSTRACT
AIM:
To establish the quality standard for Compound Kumuxiaoyan Tablets (Herba Andrographis, Ramulus et Folium Picrasmae).METHODS:
TLC was performed to identify Herba Andrographis, Ramulus et Folium Picrasmae. HPLC was used to determine deoxyandrographolide content. The Agilent ZORBAX SB C 18 column was used, and mobile phase was composed of acetonitrile 0.1%NH 3(35∶65). The detection wavelength was at 251nm.RESULTS:
The quality control study showed that the characteristic for identification by TLC was distinct and hightly specific. The quantification method of deoxyandrographolide had the linear range of 0.04992~4.992?g( r =0.9999). The average recovery was 99.70%( RSD =0.63%, n =9).CONCLUSION:
The methods of identification and quantification were accurate, realizable and reproducible. It can be used effectively for the quality control of Compound Kumuxiaoyan Tablets.
Texto completo:
DisponíveL
Índice:
WPRIM (Pacífico Ocidental)
Tipo de estudo:
Estudo diagnóstico
/
Estudo prognóstico
Idioma:
Chinês
Revista:
Chinese Traditional Patent Medicine
Ano de publicação:
1992
Tipo de documento:
Artigo
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