Simultaneous determination of 2-methoxyethyl acetate and 2-ethoxyethyl acetate in workplace air by solvent desorption-gas chromatography / 中国职业医学
China Occupational Medicine
;
(6): 211-214, 2017.
Artigo
em Chinês
| WPRIM
| ID: wpr-881601
ABSTRACT
OBJECTIVE:
To establish a solvent desorption-gas chromatography method for simultaneous determination of 2-methoxyethyl acetate(2-MEA) and 2-ethoxyethyl acetate(2-EEA) in the workplace air.METHODS:
2-MEA and 2-EEA in workplace air were captured by charcoal tubes and desorbed with solution of 5. 00%(V/V) methanol-methylene chloride,separated through capillary chromatographic column,and then analyzed by gas chromatography-flameionization detector.RESULTS:
The linear ranges of 2-MEA and 2-EEA were 1. 50-2 403. 84 and 1. 79-2 871. 20 mg/L,respectively.The correlation coefficient were 0. 999 8. The minimum quantification concentrations were 0. 20 and 0. 09 mg/m~3,respectively(3. 00 L sample). The average desorption efficiencies were 98. 08%-99. 67% and 94. 34%-99. 79%,respectively. The within-run relative standard deviations(RSD) were 1. 77%-3. 51% and 1. 72%-3. 01%,respectively.The between-run RSD were 2. 27%-4. 44% and 2. 31%-4. 19%,respectively. The samples could be stored at room temperature for at least 14 days.CONCLUSION:
This method could be used for simultaneous sampling and quantitative detection of 2-MEA and 2-EEA in workplace air.
Texto completo:
DisponíveL
Índice:
WPRIM (Pacífico Ocidental)
Idioma:
Chinês
Revista:
China Occupational Medicine
Ano de publicação:
2017
Tipo de documento:
Artigo
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