Determination of 33 inorganic elements in human hair by electricity plate digestion and inductively coupled plasma-mass spectrometry / 法医学杂志
Journal of Forensic Medicine
;
(6): 425-430, 2013.
Artigo
em Chinês
| WPRIM
| ID: wpr-983860
ABSTRACT
OBJECTIVE@#To establish the electricity plate digestion and inductively coupled plasma-mass spectrometry (ICP-MS) method for determination of 33 inorganic elements in human hair.@*METHODS@#Lithium (6Li), Germanium (72Ge), Yttrium (89Y), Indium (115In), and Terbium (159Tb) were used as internal standards. The electric heating board digestion in a mixture of nitric acid and hydrogen peroxide was used as the pre-treatment of the hair. Thirty-three inorganic elements in human hair were analyzed by ICP-MS method.@*RESULTS@#The detection limit of ICP-MS was 0.0001 microg/g(Th)-10.9 microg/g (Ca) and the limit of quantitation was 0.0005 microg/g (Th)-25 microg/g (Ca). The recovery rate of this method was 86%-113%. The RSD for the intra-day and inter-day were less than 9.2%. The method was not statistically different from microwave digestion method.@*CONCLUSION@#This method is highly efficient and accurate. It can be used for analysis of 33 inorganic elements in human hair.
Texto completo:
DisponíveL
Índice:
WPRIM (Pacífico Ocidental)
Assunto principal:
Padrões de Referência
/
Espectrometria de Massas
/
Oligoelementos
/
Sensibilidade e Especificidade
/
Eletricidade
/
Limite de Detecção
/
Cabelo
/
Micro-Ondas
Limite:
Humanos
Idioma:
Chinês
Revista:
Journal of Forensic Medicine
Ano de publicação:
2013
Tipo de documento:
Artigo
Similares
MEDLINE
...
LILACS
LIS