1.
Mol Divers
; 21(4): 925-932, 2017 11.
Article
in English
| MEDLINE
| ID: mdl-28766257
ABSTRACT
A multicomponent domino synthesis has been developed for the preparation of 2-aminopyrimidines from ß-dicarbonyl compounds, N,N-dimethylformamide dimethyl acetal, and cyanamide. The protocol was used for the regioselective preparation of 4-amide/ester/ketone substituted 2-aminopyrimidines. Twelve 2-aminopyrimidines were isolated in good yields (56-93%).
Subject(s)
Cyanamide/chemistry , Dimethylformamide/analogs & derivatives , Pyrimidines/chemistry , Pyrimidines/chemical synthesis , Catalysis , Chemistry Techniques, Synthetic , Cyclization , Dimethylformamide/chemistry , Stereoisomerism
2.
Molecules
; 14(4): 1429-37, 2009 Apr 02.
Article
in English
| MEDLINE
| ID: mdl-19384274
ABSTRACT
Novel naphtho[2,3-f]quinoxaline-2,7,12(1H)-trione and anthra-9,10-quinone dyes were synthesized in good yield from furan-2,3-diones using 1,2-diaminoanthra-9,10-quinone and 1,4-diaminoanthra-9,10-quinone. The chromophores were characterized by molecular spectroscopy methods.