ABSTRACT
Three hematite grades with different particle sizes (i.e., large, medium, and small) were evaluated, and the selection criterion was median particle size. The investigation involves the following stages: rheology, filtration, and filter cake formation. Different rheological models including Bingham, Power law, Herschel-Bulkley, and Robertson-Stiff were implemented to find the optimum model for characterizing fluid behavior. The results showed that medium-sized hematite particles produced the highest filtration volume, filter cake thickness, and filter cake permeability. These results were confirmed when a varied pore distribution filtration medium was used. The NMR results showed the same trend where the highest reduction in core porosity was found when a medium-size particle distribution was used. There is a minimum alteration in the rheological behavior of the drilling fluid as the particle size was varied, and the drilling fluids showed a shear-thinning behavior and were best described by the Herschel-Bulkley model. Particle size ratio emerges as a key factor for controlling and enhancing the filtration properties and filter cake characteristics.
ABSTRACT
Drilling fluid is a critical component in drilling operation due to its various functions. It consists of many elements, and one of the main components is the weighting material which controls the mud density. The weighting material type and concentration have a significant impact on the drilling fluid properties. A common weighting material used in the oil and gas industry is barite. In this work, the impact of barite concentration on water-based drilling fluid was evaluated. The investigated drilling fluid properties are density, pH value, filtration behavior, and rheological parameters. An intense investigation was carried out to evaluate the impact of barite concentration on the filtration and filter cake sealing properties. The density and pH values were measured at room temperature, filtration test was performed at room temperature, and differential pressure was equal to 100 psi. The rheological parameters were determined after hot rolling for 16 h at a temperature of 250 °F. The results showed that both the density and pH value increased linearly with barite dosage. The filtration volume, filter cake thickness, and permeability increased with the incremental increase in barite dosage, and the exponential relationship was the best in describing the relation with barite concentration. However, the filter cake porosity had an inverse proportional relation with barite dosage. In the case of rheological properties, all the investigated properties including the plastic viscosity, yield point, ratio of yield point to plastic viscosity, and gel strength at two different times (i.e., 10 s and 10 min) increased in general as the barite concentration increased.
ABSTRACT
A required feature of any drilling formulation is to mitigate the formation damage by having an excellent filtration and filter cake properties. The key factor for preventing and limiting formation damage is to improve the sealing qualities of the planned drilling fluid. In this study, a new novel filtration agent called "perlite" was introduced for improving the manganese tetroxide mud cake ability for better sealing features. The perlite particles were loaded to formulation containing the manganese tetroxide as weighting agent. The water-based drilling mud was designed at high densities (14.25 and 17.2 ppg). Perlite was added in varied concentrations to reach the optimum performance. The filtration test conducted at reservoir temperature of 250 °F and a differential pressure of 300 psi to form the filter cake. The tests were performed using sandstone cores with two different permeability categories (low and high permeabilities) as the filtration media. This gave the full picture of perlite performance as implemented for different formation properties and considering the drilling fluid properties. The formed filter cake structure and chemical composition was evaluated using scanning electron energy-dispersive X-ray (SEM-EDS). The presented results illustrated how the perlite was compatible to be added to the manganese tetroxide weighting agents in the same formulation. In addition, it has the capacity to improve the filter cake's sealing qualities, lowering the filtration volume by 41% and the filter cake internal and external layers permeability by 58% and 25%, respectively. Moreover, the EDS analysis showed that the perlite particles are concentrated generally in the internal layer of the filter cake.
Subject(s)
Filtration , Manganese , Filtration/methods , Aluminum Oxide/chemistry , PermeabilityABSTRACT
The hydrate formation during the transportation and injection of carbon dioxide in pipelines always leads to the risk of plugging. The development of a cost-efficient CO2 sequestration method requires efficient hydrate inhibitors. In this research work, the synthesized carbon quantum dots (CQDs) of monoethylene glycol (MEG) were tested with CO2 hydrates for their hydrate inhibition efficiency. The hydrothermal method was used for the synthesis of CQDs. The synthesized CQDs were characterized using UV light (365 nm), UV-vis absorption, Fourier transform infrared spectroscopy (FTIR), transmission electron microscopy (TEM), and photoluminescence (PL) spectroscopy. MEG CQDs were found to have very good water solubility and fluorescence properties. The MEG CQDs were tested for their CO2 hydrate inhibition efficiency using the sapphire rocking cell unit. Test results proved that MEG CQDs are much more effective as a CO2 hydrate inhibitor in comparison to MEG.
