Effect from Autoclave Sterilization and Usage on the Fracture Resistance of Heat-Treated Nickel-Titanium Rotary Files.

This study aimed to assess the effect of mechanical loading and heating on the cyclic fatigue and torsional fracture resistances of heat-treated nickel-titanium files after usage and autoclaving. Sixty files (One Curve) were tested for cyclic fatigue and torsional fracture resistances using customized devices. The files were divided into three groups according to the test conditions (n = 10); new (group-N), used for simulated canal shaping (group-U), and sterilized after use (group-S). For cyclic fatigue resistances, the files were freely rotated in a curved metal canal under body temperature; the time elapsed to fracture was recorded and the numbers of cycles to fracture (NCF) were calculated. For the torsional resistances, the file tip was fixed and rotated until the file fractured. The maximum torsional load and distortion angle were recorded. The toughness was calculated. Fracture fragments were examined with a scanning electron microscope. Data were analyzed using a one-way analysis of variance and Tukey's post hoc test at the significance level of 95%. Group-U showed significantly higher NCF than group-S (p < 0.05). However, there was no significant differences between groups-N and -S in the NCF (p > 0.05). Group-N showed a significantly bigger distortional angle and higher torsional toughness than groups-U and -S, but the ultimate torsional strength did not have significant difference between the groups. Under the limitation of this study, autoclave sterilization after single-usage did not improve the fracture resistance of heat-treated One Curve nickel-titanium files.

Fracture Resistance of Heat-Treated Nickel-Titanium Rotary Files After Usage and Autoclave Sterilization: An In Vitro Study.

INTRODUCTION: This study aimed to evaluate the dynamic cyclic fatigue resistance of heat-treated nickel-titanium (NiTi) files after usage and autoclaving. METHODS: Two heat-treated NiTi file systems with tip sizes of #25 (ie, ProTaper Gold F2 [Dentsply Sirona, Charlotte, NC] and TruNatomy Prime [Dentsply Sirona]) were selected. Files of each system were divided into 3 experimental subgroups (n = 10). For subgroup 1, new files were tested to establish the baseline number of cycles to failure (NCF). For subgroup 2, files underwent canal instrumentation in a simulated J-shaped canal block with 35° of curvature and a 16.5-mm length. The simulated canals were pre-enlarged using stainless steel files #10K and #15K. After instrumentation, the files were tested. For subgroup 3, files underwent canal instrumentation as in subgroup 2 followed by autoclave sterilization and then were tested for cyclic failure. The cyclic fatigue test was performed in dynamic pecking motion under body temperature. The time to fracture was recorded and calculated into NCF. Fracture fragment lengths were measured using a digital microcaliper. Statistical analysis was conducted using the independent t test and multifactorial analysis of variance with 95% significance. Scanning electron microscopy was used to examine the topographic characteristics after cyclic fatigue tests. RESULTS: There were no significant differences between file systems in subgroup 1 using new files (P < .05). Although PG reduced the NCF after use, TN showed a significantly increased NCF (P < .05). However, after sterilization, TN showed a reduced NCF compared with the used one (P < .05). CONCLUSIONS: Cyclic loading by usage and heat treatment during sterilization may result in different cyclic fatigue resistance according to the geometry and alloy characteristics.

Mechanical Properties of Glide Path Preparation Instruments with Different Pitch Lengths.

INTRODUCTION: This study compared the effects of pitch length on the torsional resistance and cyclic fatigue resistance of glide path preparation instruments. METHODS: G-File (G1 and G2; Micro-Mega, Besançon, France) and new generation G-File (NG1 and NG2, Micro-Mega) instruments were compared to evaluate the effects of the shorter pitch of the latter (25% shorter than G-File). G1 and NG1 have a #12 tip size, whereas G2 and NG2 have a #17 tip size. All the files have the same taper of 3%. For comparing the torsional resistances (n = 15), the file was fixed at 4 mm from the tip, and the clockwise rotation at a constant rotational speed of 2 rpm was adjusted until the file fractured. The maximum torsional load and distortion angle at fracture were recorded. For comparing the cyclic fatigue resistances (n = 15), the files were freely rotated in a simulated canal (radius, 3 mm; curvature, 90°) at a speed of 300 rpm in a dynamic mode. When the file fractured, the time elapsed was recorded using a chronometer. The number of cycles to failure was calculated by multiplying the total time to failure by the rotation rate. Fractured fragments were examined under the scanning electron microscope. RESULTS: The NG2 instruments had significantly higher fatigue resistance and torsional strength than the G2 instruments (P < .05) and showed approximately the same fatigue resistance as the G1. Scanning electron microscopic examinations revealed the typical appearances of 2 failure modes. CONCLUSIONS: A shorter pitch design increased cyclic fatigue resistance and torsional strength of the glide path instruments.