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1.
J Appl Crystallogr ; 55(Pt 4): 919-928, 2022 Aug 01.
Article in English | MEDLINE | ID: mdl-35974731

ABSTRACT

A systematic study has been carried out to investigate the neutron transmission signal as a function of sample tem-per-ature. In particular, the experimentally de-ter-mined wavelength-dependent neutron attenuation spectra for a martensitic steel at tem-per-atures ranging from 21 to 700°C are com-pared with simulated data. A theoretical description that includes the Debye-Waller factor in order to describe the tem-per-ature influence on the neutron cross sections was im-plemented in the nxsPlotter software and used for the simulations. The analysis of the attenuation coefficients at varying tem-per-atures shows that the missing contributions due to elastic and inelastic scattering can be clearly distinguished: while the elastically scattered intensities decrease with higher tem-per-atures, the inelastically scattered intensities increase, and the two can be separated from each other by analysing unique sharp features in the form of Bragg edges. This study presents the first systematic approach to qu-antify this effect and can serve as a basis , for example, to correct measurements taken during in situ heat treatments, in many cases being a prerequisite for obtaining qu-anti-fiable results.

2.
Rev Sci Instrum ; 90(12): 125108, 2019 Dec 01.
Article in English | MEDLINE | ID: mdl-31893786

ABSTRACT

In various kinds of radiography, deficient transmission imaging may occur due to backlighting inside the detector itself arising from light or radiation scattering. The related intensity mismatches barely disturb the high resolution contrast, but its long range nature results in reduced attenuation levels which are often disregarded. Based on X-ray observations and an empirical formalism, a procedure is developed for a first order correction of detector backlighting. A backlighting factor is modeled as a function of the relative detector coverage by the sample projection. Different cases of sample transmission are regarded at different backlight factors and detector coverage. The additional intensity of backlighting may strongly affect the values of materials' attenuation up to a few 10%. The presented scenario provides a comfortable procedure for corrections of X-ray or neutron transmission imaging data.

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