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1.
Materials (Basel) ; 17(2)2024 Jan 21.
Article in English | MEDLINE | ID: mdl-38276453

ABSTRACT

The low-temperature impact toughness of nodular cast iron can be significantly enhanced by heat treatment, and thus meet the severe service requirements in the fields of high-speed rail and power generation, etc. In order to explore the enhancement mechanism, microstructure, hardness, composition and other characteristics of as-cast and heat-treated nodular cast iron is systematically tested and compared by optical microscopy, microhardness tester, EBSD, SEM, electron probe, and impact toughness testing machine in this study. The results show that heat treatment has little effect on the morphology and size of graphite in nodular cast iron, ignores the effect on the grain size, morphology, and distribution of ferritic matrix, and has little effect on the hardness and exchange of elements, while it is meaningful to find that heat treatment brings about significant decrease in high-angle grain boundaries (HAGB) between 59° and 60°, decreasing from 10% to 3%. Therefore, the significant enhancement of low-temperature impact toughness of nodular cast iron by heat treatment may result from the obvious decrease in HAGB between 59° and 60°, instead of other reasons. From this perspective, the study can provide novel ideas for optimizing the heat treatment process of nodular cast iron.

2.
Materials (Basel) ; 16(6)2023 Mar 07.
Article in English | MEDLINE | ID: mdl-36984032

ABSTRACT

The welding titanium cathode roller has the obvious advantages of low cost, high efficiency, and no diameter restriction. Unfortunately, the longitudinal weld on the cathode roller adversely impacts the quality of the electrolytic copper foil due to the great difference between the microstructure of the weld zone and the base metal. Thus, it is crucial to reduce their difference by regulating the microstructure of the weld zone. In this study, a novel complex treatment of heat treatment and sandblasting is primarily developed for regulating the microstructure of the weld zone. The results show that the novel complex treatment has an efficient effect on regulating the microstructure of the weld zone and making the microstructure in the weld zone close to that of the base metal. During vacuum annealing, the microstructure of the weld zone is refined to some degree, and 650 °C annealing has the optimal effect, which can effectively reduce the ratio of α phase's length to width and reduce the microstructure difference between the weld zone and the base metal. At the same time, with an increase in the annealing temperature, the tensile strength and yield strength decreased by about 10 MPa; the elongation after fracture increased by 20%; the average microhardness of the WZ and the HAZ decreased by about 10 HV0.10; and that of the BM decreased by about 3 HV0.10. The heat treatment after welding can effectively adjust the properties of the weld zone, reduce the hardness and strength, and improve the toughness. The subsequent sandblasting after annealing can further refine the grain size in the weld zone and make the microstructure in the weld zone close to that of the base metal. Sandblasting after annealing can further refine the grain in the weld zone and make the microstructure in the weld zone close to that of base metal. Meanwhile, an application test confirmed that the adverse impact of a longitudinal weld on the quality of electrolytic copper foil could be resolved by adopting this novel complex treatment. Therefore, this study provides valuable technical support for the "welding" manufacturing of the titanium sleeves of the cathode roller.

3.
Materials (Basel) ; 15(4)2022 Feb 17.
Article in English | MEDLINE | ID: mdl-35208033

ABSTRACT

Changes in the texture as well as mechanical properties of CoNiFeV0.5Mo0.2 medium entropy alloy wire rods during loading-unloading are investigated. The intensity of the recrystallization texture {001}<110> component and fraction of low angle grains increase with the loading-unloading cycles and the alloy strength increases (934 MPa to 1083 MPa) due to dislocation increment in the loading-unloading cycles. The loading modulus (El) and average modulus (Esecant) for a hysteresis loop decrease slightly, whereas the unloading modulus (Eun) increases, the Eun increment of 5-TC-UTand 10-TC-UT are 22 and 137 GPa.

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