1.
Acta Crystallogr Sect E Struct Rep Online
; 69(Pt 8): o1308-9, 2013.
Article
in English
| MEDLINE
| ID: mdl-24109383
ABSTRACT
The absolute configuration of the title compound, C16H26O, was determined as (1R,3S,8R,11R) based mainly on the synthetic pathway but is also implied by the X-ray analysis. The mol-ecule contains fused six- and seven-membered rings. Part of the seven-membered ring was refined as disordered over two sets of sites with the occupancy ratio fixed at 0.86:0.14. The disorder corresponds to a major chair conformation and a minor boat conforation. In the crysyal, O-Hâ¯O hydrogen bonds connect the mol-ecules into chains parallel to the a axis.