Your browser doesn't support javascript.
loading
Show: 20 | 50 | 100
Results 1 - 6 de 6
Filter
Add more filters










Database
Language
Publication year range
1.
Forensic Sci Int Synerg ; 8: 100465, 2024.
Article in English | MEDLINE | ID: mdl-38596784

ABSTRACT

The use of collaborative exercises (CE) and proficiency tests (PT) as part of the governance programme for any forensic science laboratory has become commonplace and recommended by several international organisations. Traditionally these have been discipline-specific exercises testing a laboratory's ability in a single area of forensic science. However, the "real" world is normally more complex and, in many instances, forensic material must be examined for a number of different evidence types. This article summarises the concepts, planning, design, preparation, implementation, co-ordination and evaluation of the 2022 Multidisciplinary Collaborative Exercise (2022-MdCE) covering a range of forensic disciplines, specifically DNA, fingerprint, documents and handwriting. The exercise consisted of a questioned letter with typescript text and a signature. In addition, the letter contained a visible bloody fingermark in the area of the signature, a visible staining in the lower left-hand corner, a latent fingermark and an indented impression. The analysis of the results showed that, in the investigation of the bloody fingermark, the priority was given to the DNA examination. Some critical issues emerged in relation to the biological (DNA)/ink sampling strategies when applied before fingermark visualisation. Another outcome of the exercise has been to demonstrate the importance of indented impressions, which have been underestimated by a significant number of participants. As setters, more in-depth studies are needed to produce consistent samples. This concerns all the disciplined involved but especially DNA and fingermarks. Based on this exercise, it is believed that this approach to testing of forensic disciplines allows the analysis of good practice within the various scientific areas, as well as scrutinising the process and sequence of events for examining the material within a forensic laboratory in the best conservative way for all kind of evidences.

2.
Sci Justice ; 62(5): 556-568, 2022 09.
Article in English | MEDLINE | ID: mdl-36336449

ABSTRACT

Previous studies have identified the potential benefit of the disulfur dinitride (S2N2) process to operationally relevant substrates. However, the majority of this work was conducted on prototype equipment that had substantial differences to the commercialised system (Recover Latent Fingerprint Technology (LFT)) in terms of design and chemical delivery. This paper evaluates the performance of Recover LFT on a problematic exhibit encountered within a fingerprint enhancement laboratory: unfired and fired ammunition. Three pseudo-operational experiments involving non-groomed, naturally handled fingermarks were conducted on the most commonly encountered types of ammunition used in crime in the United Kingdom (UK). In addition, Recover LFT was compared against Superglue Fuming followed by Basic Yellow 40 (BY40) Fluorescent Dye Staining (a commonly used alternative) to ascertain if the process provides added benefit to fingermark recovery rates. The results show that fingermark visualisation on small calibre cartridge cases remains difficult with few marks achieving enough ridge detail for comparison. However, this paper also shows that the novel Recover LFT process, which is still in its infancy and requiring optimisation, is no worse than currently implemented visualisation processes and is therefore worth further investigation.


Subject(s)
Dermatoglyphics , Firearms , Humans , Cyanoacrylates , Fluorescent Dyes , Technology
3.
Sci Justice ; 52(3): 145-60, 2012 Sep.
Article in English | MEDLINE | ID: mdl-22841138

ABSTRACT

Currently there is no standard way of carrying out research into finger mark enhancement techniques. Individuals, groups or establishments tend to use different methodologies depending on a number of factors, especially finance and time. However, data published in the literature can be misleading to the forensic community if the data generated reflects research involving very few finger marks or if those finger marks have been deliberately doped with an unnatural balance of sweat or an unusual contaminant. This paper presents an experimental methodology which is intended to establish minimum standards for those carrying out finger mark enhancement research (at least within the United Kingdom) and bring some consistency to the process. It will aim to identify the many variables encountered when dealing with finger marks and suggest experimental methods to take these into account. It will also present the key stages of the progression of a process from a laboratory concept to a tool used on operational work.


Subject(s)
Dermatoglyphics , Eccrine Glands , Humans , Indicators and Reagents , Sebaceous Glands , Spectrometry, Fluorescence , Surface Properties , Volatilization
4.
Forensic Sci Int ; 212(1-3): 130-42, 2011 Oct 10.
Article in English | MEDLINE | ID: mdl-21719220

ABSTRACT

Research has been conducted to establish the effect that changes in relative humidity have on both the effectiveness of the cyanoacrylate fuming technique and the microstructures formed by the polymerisation reaction during the development of the marks. The study investigated 'natural' fingermarks and deliberately groomed eccrine and sebaceous marks, all exposed to relative humidity levels in the range 60-100%. It was found that the optimum level of relative humidity for the development of the most high quality marks is approximately 80%, in accord with current recommendations for operational implementation which are based on previous unpublished work. The eccrine constituents of the fingerprints are most influenced by humidity changes. Three humidity regimes were identified, each giving different polycyanoacrylate microstructures. Humidity levels of 60% give flat, film-like structures whereas in the range 70-90% the characteristic noodle-like structure is formed. At higher humidities, thin, flat thread-like growth is observed with some 'collapsed sphere' structures observed close to pores and significant background development. The noodle-like structures are thought to scatter more light and retain fluorescent dye better than the structures formed at other humidity levels. Sebaceous marks produce a very different polymer microstructure, resembling a flat film with some fine nodular structures.


Subject(s)
Cyanoacrylates/chemistry , Dermatoglyphics , Humidity/adverse effects , Forensic Medicine/methods , Humans , Materials Testing , Sensitivity and Specificity , Specimen Handling , Structure-Activity Relationship , Trace Elements , Volatilization
5.
Anal Chem ; 72(1): 141-9, 2000 Jan 01.
Article in English | MEDLINE | ID: mdl-10655646

ABSTRACT

We derive a lumped-element, equivalent-circuit model for the thickness-shear mode (TSM) resonator with a viscoelastic film. This modified Butterworth-Van Dyke model includes in the motional branch a series LCR resonator, representing the quartz resonance, and a parallel LCR resonator, representing the film resonance. This model is valid in the vicinity of film resonance, which occurs when the acoustic phase shift across the film is an odd multiple of pi/2 rad. For low-loss films, this model accurately predicts the frequency changes and damping that arise at resonance and is a reasonable approximation away from resonance. Elements of the parallel LCR resonator are explicitly related to film properties and can be interpreted in terms of elastic energy storage and viscous power dissipation. The model leads to a simple graphical interpretation of the coupling between the quartz and film resonances and facilitates understanding of the resulting responses. These responses are compared with predictions from the transmission-line and Sauerbrey models.


Subject(s)
Electrochemistry/methods , Elasticity , Electric Impedance , Electrochemistry/instrumentation , Electrodes , Quartz , Surface Properties , Viscosity
6.
Anal Chem ; 71(11): 2205-14, 1999 Jun 01.
Article in English | MEDLINE | ID: mdl-21662758

ABSTRACT

We develop a general model that describes the electrical responses of thickness-shear mode resonators subject to a variety of surface conditions. The model incorporates a physically diverse set of single-component loadings, including rigid solids, viscoelastic media, and fluids (Newtonian or Maxwellian). The model allows any number of these components to be combined in any configuration. Such multiple loadings are representative of a variety of physical situations encountered in electrochemical and other liquid-phase applications, as well as gas-phase applications. In the general case, the response of the composite load is not a linear combination of the individual component responses. We discuss application of the model in a qualitative diagnostic fashion to gain insight into the nature of the interfacial structure, and in a quantitative fashion to extract appropriate physical parameters such as liquid viscosity and density and polymer shear moduli.

SELECTION OF CITATIONS
SEARCH DETAIL
...