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1.
Materials (Basel) ; 17(11)2024 May 21.
Article in English | MEDLINE | ID: mdl-38893741

ABSTRACT

Injection molding technology is widely utilized across various industries for its ability to fabricate complex-shaped components with exceptional dimensional accuracy. However, challenges related to injection quality often arise, necessitating innovative approaches for improvement. This study investigates the influence of surface roughness on the efficiency of conformal cooling channels produced using additive manufacturing technologies, specifically Direct Metal Laser Sintering (DMLS) and Atomic Diffusion Additive Manufacturing (ADAM). Through a combination of experimental measurements, including surface roughness analysis, scanning electron microscopy, and cooling system flow analysis, this study elucidates the impact of surface roughness on coolant flow dynamics and pressure distribution within the cooling channels. The results reveal significant differences in surface roughness between DMLS and ADAM technologies, with corresponding effects on coolant flow behavior. Following that fact, this study shows that when cooling channels' surface roughness is lowered up to 90%, the reduction in coolant media pressure is lowered by 0.033 MPa. Regression models are developed to quantitatively describe the relationship between surface roughness and key parameters, such as coolant pressure, Reynolds number, and flow velocity. Practical implications for the optimization of injection molding cooling systems are discussed, highlighting the importance of informed decision making in technology selection and post-processing techniques. Overall, this research contributes to a deeper understanding of the role of surface roughness in injection molding processes and provides valuable insights for enhancing cooling system efficiency and product quality.

2.
Materials (Basel) ; 17(11)2024 Jun 03.
Article in English | MEDLINE | ID: mdl-38893982

ABSTRACT

Rubber blends based on styrene-butadiene rubber, ethylene-propylene-diene monomer rubber and a combination of both rubbers were cured with different sulfur and peroxide curing systems. In sulfur curing systems, two type of accelerators, namely tetramethylthiuram disulfide, N-cyclohexyl-2-benzothiazole sulfenamide, and combinations of both accelerators were used. In peroxide curing systems, dicumyl peroxide, and a combination of dicumyl peroxide with zinc diacrylate or zinc dimethacrylate, respectively, were applied. The work was aimed at investigating the effect of curing systems composition as well as the type of rubber or rubber combinations on the curing process, cross-link density and physical-mechanical properties of vulcanizates. The dynamic mechanical properties of the selected vulcanizates were examined too. The results revealed a correlation between the cross-link density and physical-mechanical properties. Similarly, there was a certain correlation between the cross-linking degree and glass transition temperature. The tensile strength of vulcanizates based on rubber combinations was higher when compared to that based on pure rubbers, which points out the fact that in rubber combinations, not only are the features of both elastomers combined, but improvement in the tensile characteristics can also be achieved. When compared to vulcanizates cured with dicumyl peroxide, materials cured with a sulfur system exhibited higher tensile strength. With the application of co-agents in peroxide vulcanization, the tensile strength overcame the tensile behavior of sulfur-cured vulcanizates.

3.
Polymers (Basel) ; 16(4)2024 Feb 06.
Article in English | MEDLINE | ID: mdl-38399828

ABSTRACT

The modification of polymer materials' useful properties can be applicable in many industrial areas due to the ability to make commodity and technical plastics (plastics that offer many benefits, such as processability, by injection molding) useful in more demanding applications. In the case of injection-molded parts, one of the most suitable methods for modification appears to be high-energy irradiation, which is currently used primarily for the modification of mechanical and thermal properties. However, well-chosen doses can effectively modify the properties of the surface layer as well. The purpose of this study is to provide a complex description of high-energy radiation's (ß radiation) influence on the useful properties of injection-molded parts made from common polymers. The results indicate that ß radiation initiates the cross-linking process in material and leads to improved mechanical properties. Besides the cross-linking process, the material also experiences oxidation, which influences the properties of the surface layer. Based on the measured results, the main outputs of this study are appropriately designed regression models that determine the optimal dose of radiation.

4.
Materials (Basel) ; 16(6)2023 Mar 16.
Article in English | MEDLINE | ID: mdl-36984271

ABSTRACT

Nowadays, technical practice puts emphasis on improving selected material properties of polymers which could lead to new applications. Material properties can be modified in numerous ways, among which is radiation treatment. This study looks into the influence of beta radiation on several properties of polyamide 6, e.g., indentation hardness, modulus and creep. Main changeable parameters were the concentration of triallyl isocyanurate (TAIC), which promotes cross-linking, and intensity of radiation. The concentration was in the range from 2 to 6 wt.%, while the radiation dose was 0, 66, 99 and 132 kGy. The treated materials were measured for indentation hardness, modulus and creep. Degree of cross-linking was verified by thermo-mechanical analysis (TMA), while degradation processes was investigated by Fourier-transform infrared spectroscopy (FTIR). The results indicate that electron radiation positively affects the tested material properties. The best results were seen in polyamide with 6 wt.% of TAIC, which demonstrated a 38% improvement in mechanical properties after exposure to 132 kGy. This improvement in properties affects the final parts and their application (e.g., in the automotive industry-engine parts; in electrical engineering-insulation of wires and cables; and in industry-pipes for underfloor heating, etc.).

5.
Sensors (Basel) ; 24(1)2023 Dec 24.
Article in English | MEDLINE | ID: mdl-38202959

ABSTRACT

The main object of this research was to develop a security system to evaluate the intrusion into an object through a glass pane. More specifically, this study deals with sensing and evaluating signals from a contact glass-break detector, which is part of an intruder alarm system. Each alarm detector in an alarm system must accomplish certain security level requirements that strictly describe the requirements for the area of use and the detector's reliability. To date, no contact glass-break detector has been developed and fully tested to meet the stringent requirements of the highest security level. A contact glass-break detector was developed whose main part is an accelerometer that transmits signals from the glass pane. These signals were evaluated according to the developed methodology. It was verified that the proposed system can distinguish at the highest security level between false alarms and situations where the building has been intruded.

6.
Materials (Basel) ; 14(1)2020 Dec 25.
Article in English | MEDLINE | ID: mdl-33375751

ABSTRACT

The goal of this research was to examine the effect of two surface modification methods, i.e., radiation cross-linking and plasma treatment, on the adhesive properties and the final quality of adhesive bonds of polypropylene (PP), which was chosen as the representative of the polyolefin group. Polymer cross-linking was induced by beta (accelerated electrons-ß-) radiation in the following dosages: 33, 66, and 99 kGy. In order to determine the usability of ß- radiation for these applications (improving the adhesive properties and adhesiveness of surface layers), the obtained results were compared with values measured on surfaces treated by cold atmospheric-pressure plasma with outputs 2.4, 4, and 8 W. The effects of both methods were compared by several parameters, namely wetting contact angles, free surface energy, and overall strength of adhesive bonds. Furthermore, Fourier transform infrared (FTIR) spectroscopy and scanning electron microscopy (SEM) were conducted. According to our findings the following conclusion was reached; both tested surface modification methods significantly altered the properties of the specimen's surface layer, which led to improved wetting, free surface energy, and bond adhesion. Following the ß- radiation, the free surface energy of PP rose by 80%, while the strength of the bond grew in some cases by 290% in comparison with the non-treated surface. These results show that when compared with cold plasma treatment the beta radiation appears to be an effective tool capable of improving the adhesive properties and adhesiveness of PP surface layers.

7.
Materials (Basel) ; 13(4)2020 Feb 19.
Article in English | MEDLINE | ID: mdl-32093045

ABSTRACT

This study's goal was to describe the influence of a wide range of ionizing beta radiation upon the changes in surface layer mechanical properties and structural modifications of selected types of polymer. Radiation crosslinking is a process whereby the impingement of high-energy electrons adjusts test sample structures, thus enhancing the useful properties of the material, e.g., hardness, wear-resistance, and creep, in order that they may function properly during their technical use. The selected polymers tested were polyolefin polymers like polyethylene (Low-density polyethylene LDPE, High-density polyethylene HDPE). These samples underwent exposure to electron radiation of differing dosages (33, 66, 99, 132, 165, and 198 kGy). After the crosslinking process, the samples underwent testing of the nano-mechanical properties of their surface layers. This was done by means of a state-of-the-art indentation technique, i.e., depth-sensing indentation (DSI), which detects the immediate change in the indentation depth associated with the applied force. Indeed, the results indicated that the optimal radiation dosage increased the mechanical properties by up to 57%; however, the beneficial levels of radiation varied with each material. Furthermore, these modifications faced examination from the structural perspective. For this purpose, a gel test, Raman spectroscopy, and crystalline portion determination by X-ray all confirmed the assumed trends.

8.
Polymers (Basel) ; 11(11)2019 Nov 12.
Article in English | MEDLINE | ID: mdl-31726648

ABSTRACT

Bonding is increasingly being used, and it is an ever-evolving method for creating unbreakable bonds. The strength of adhesive bonds determines, to a significant extent, the possible applications of this technology and is influenced by many factors. In addition to the type of adhesive used, the characteristics of the surface layers play a significant role; therefore, significant attention is paid to their adjustment and modification. Radiation crosslinking is one of the most important methods for modifying polymer properties. Currently, the most frequently used type of radiation for polymer crosslinking is beta minus (ß-) radiation, which affects not only mechanical but also surface properties, chemical and temperature resistance, and surface layer characteristics of polymers. This study investigated the effect of ß- radiation on the surface layer properties of low-density polyethylene (LDPE), high-density polyethylene (HDPE), and polypropylene (PP) and the effects of surface-layer modification on the ultimate tensile strength of bonded joints. Based on the results, we concluded that ß- radiation significantly changes the properties of the tested surface layers, increases the surface energy, and improves the adhesiveness of bonds. Consequently, the final strength of the LDPE, HDPE, and PP bonds increases significantly.

9.
Polymers (Basel) ; 10(2)2018 Feb 07.
Article in English | MEDLINE | ID: mdl-30966194

ABSTRACT

This article deals with the influence of electron-beam radiation on the micro-mechanical, thermo-mechanical, and structural properties of selected polymers. In the search for the desired improvement of polymers, it is possible to use, inter alia, one particular possible modification-Namely, crosslinking-Which is a process during which macromolecular chains start to connect to each other and, thus, create the spatial network in the structure. In the course of the treatment of the ionizing radiation, two actions can occur: crosslinking and scission of macromolecules, or degradation. Both these processes run in parallel. Using the crosslinking technology, standard and technical polymers can acquire the more "expensive" high-tech polymeric material properties and, thus, replace these materials in many applications. The polymers that were tested were selected from across the whole spectra of thermoplastics, ranging from commodity polymers, technical polymers, as well as high-performance polymers. These polymers were irradiated by different doses of beta radiation (33, 66, 99, 132, 165, and 198 kGy). The micro-mechanical and thermo-mechanical properties of these polymers were measured. When considering the results, it is obvious that irradiation acts on each polymer differently but, always when the optimal dose was found, the mechanical properties increased by up to 36%. The changes of micro-mechanical and thermo-mechanical properties were confirmed by structural measurement when the change of the micro-hardness and modulus corresponded to the crystalline phase change as determined by X-ray and gel content.

10.
ScientificWorldJournal ; 2013: 454710, 2013.
Article in English | MEDLINE | ID: mdl-23844398

ABSTRACT

The paper deals with the influence of soil genesis on the physical-mechanical properties. The presented case study was conducted in the region of the Ostrava Basin where there is a varied genetic composition of the Quaternary geological structure on the underlying Neogeneous sediments which are sediments of analogous granulometry but different genesis. In this study, 7827 soil samples of an eolian, fluvial, glacial, and deluvial origin and their laboratory analyses results were used. The study identified different values in certain cases, mostly in coarser-grained foundation soils, such as sandy loam S4 (MS) and clayey sand F4 (CS). The soils of the fluvial origin manifest different values than other genetic types. Next, based on regression analyses, dependence was proved neither on the deposition depth (depth of samples) nor from the point of view of the individual foundation soil classes or the genetic types. The contribution of the paper is to point at the influence of genesis on the foundation soil properties so that engineering geologists and geotechnicians pay more attention to the genesis during engineering-geological and geotechnical investigations.


Subject(s)
Geologic Sediments/analysis , Geologic Sediments/chemistry , Soil/analysis , Soil/chemistry , Compressive Strength , Materials Testing , Particle Size , Surface Properties
11.
ScientificWorldJournal ; 2013: 529431, 2013.
Article in English | MEDLINE | ID: mdl-24391464

ABSTRACT

This study deals with a methodical identification and evaluation of physical-mechanical properties of one genetic type of geological structure. This is represented by an engineering-geological zone of eolian sediments, which is regionally rather abundant. The paper contributes to a need to identify typical soil properties for widespread geological environments in a particular region and thus add to good engineering geologists and geotechnical engineers' awareness in the region. Such information is much required as it permits comparing results of newly conducted engineering-geological investigations and research with the results characteristic for the region in question. It is vital for engineering geologists and geotechnical engineers to be sufficiently informed on the foundation soil properties of widespread geological environments because of professionalism and higher quality of their work results. Comparing other loess sediment studies worldwide it was discovered that the physical properties of the most abundant clays of low to medium plasticity, sandy clays, and sands as foundation soils vary as for the plasticity index, porosity, natural water content, and bulk density to a certain extent but not as significantly as once expected.


Subject(s)
Geologic Sediments , Aluminum Silicates/analysis , Clay , Czech Republic , Geologic Sediments/chemistry , Soil/chemistry
12.
Environ Monit Assess ; 184(11): 6709-33, 2012 Nov.
Article in English | MEDLINE | ID: mdl-22134855

ABSTRACT

Underground mining activities may potentially play a role on the initiation and reactivation of the slope movements. However, an adequate attention has not yet been paid to these problems; in this study, the possible influence of present and former mining activities on the selected set of model slope deformations in the Ostrava-Karviná Coalfield (Opliji, Repiste and Orlova Lazy District) was analysed and a methodology for their observation for application to similar conditions and influence was described. Isocatabase maps, terrain deformation parameters calculated for the point lying on the slope deformation surface, length measurement by zone extensometer and dilatometer measurement in cracks was also provided for evaluation of the underground mining impact. It was found that inclinations of both boreholes were evidence of underground mining impact, and localization of inclinometer measurement on boreholes in the active part as well as in the near vicinity was very important as an important result of this study. Analysis of underground mining activity influence on model localities in relation to performed mining operations, subsidence and other influences on the ground surface was also determined. Thus, the study will contribute to a more objective knowledge of these problems of interest for the professional public and also for the state administration to solve problems associated with the utilisation and settlement of such affected areas.


Subject(s)
Coal Mining , Environmental Monitoring , Geological Phenomena , Czech Republic
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