Reflectivity and scattering measurements of an Advanced X-ray Astrophysics Facility test coating sample.

Reflectivity and scattering profile measurements were made on a gold-coated witness sample produced to evaluate mirror coatings for the Advanced X-ray Astrophysics Facility program. Reflectivity measurements were made at Al K, Ti K, and Cu K energies as a function of incident graze angle. The results are fit to a model that includes the effects of roughness, particulate and organic contamination layers, and gold-coating density. Reflectivities are close to theoretical, with the difference being well accounted for by 4.1 Å of roughness at spatial frequencies above 4 µm(-1), a gold-coating density equal to 0.98 bulk, and a surface contaminant layer 27 Å thick. Scattering measurements extending to ±35 arcmin of the line center were obtained by the use of Al K x rays and incidence angles from 0.75° to 3°. The scattering profiles imply a power spectral density of surface-scattering frequencies that follows a power law with an index of -1.0 and a total surface roughness for the spatial frequency band between 0.05 µm(-1) and 4 µm(-1) of 3.3 Å Combining the roughnesses derived from both the reflectivity and scattering measurements yields a total roughness of 5.3 Å for scattering frequencies between 0.05 µm(-1) and 15,000 µm(-1).

A high galactic latitude survey of far-ultraviolet excess objects.

Optical spectra have been obtained for a selection of objects included in a catalog of far ultraviolet bright, high galactic latitude objects detected with a balloon-borne survey telescope. The observed objects provide a sample of subdwarf O and B stars, white dwarfs, and binary systems including a hot subluminous member. Model atmospheres analysis of the subdwarf sample is used to determine the temperature, gravity, and helium to hydrogen ratio of the individual objects. A smooth distribution of objects is found on the gravity versus temperature diagram near the theoretical location of the extended horizontal branch. A break between the helium rich and helium poor objects occurs at 40,000 K. Suspected binary objects were found and analyzed to determine the temperature and gravity of the hot subluminous member in each system. The number of subdwarf stars contained in binaries is determined to be from 65% to 100%. The number versus ultraviolet magnitude distribution of the subdwarf B sample is modeled to obtain a midplane density of 3.3 10(-6) pc-3 and a population scale height of 240 pc. The proportion of white dwarfs that experience the subdwarf phase of evolution is found to be 0.94%.

Copper determination in urine by flow injection analysis with electrochemical detection at platinum disk microelectrodes of various radii.

The incorporation of platinum disk microelectrodes of various radii (2.5-50 microns) in a well-jet flow cell offers reduced limits of detection for the determination of copper in urine by flow injection analysis compared with standard methods based on a conventional sized glassy carbon disk macroelectrode (radius 1.5 mm), in a thin-layer cell. The radius of the platinum disk microelectrode was found to be critical with respect to both the limit of detection and flow rate dependence. An optimal radius value of 28 microns was found with detection limits increasing with both larger and smaller electrode radii. In contrast, as theoretically expected, a diminished flow rate dependence was observed the smaller the radii of the platinum disk microelectrodes. Sample cleanup and preparation is conveniently achieved by the use of Sep-Pak cartridges and formation of a copper dithiocarbamate complex. The metal complex is easily oxidized at platinum disk microelectrodes in acetonitrile, which was the solvent used in the flow injection method of analysis.

Astronomical observations with the FAUST telescope.

The far-ultraviolet space telescope (FAUST) was flown on Spacelab 1 to provide wide-field imaging in the wavelength range 1300 to 1800 angstroms. Most of the developed film showed high levels of background exposure. Frames with a lower background included exposures of the Cygnus Loop supernova remnant and an exposure in the direction of the galaxy cluster Abell 2634. Several exposures will be used in a search for hot white dwarf stars.