ABSTRACT
In this work we present a novel route to produce a graphene-based film on a polymer substrate. A transparent graphite colloidal suspension was applied to a slat of poly(methyl methacrylate) (PMMA). The good adhesion to the PMMA surface, combined with the shear stress, allows a uniform and continuous spreading of the graphite nanocrystals, resulting in a very uniform graphene multilayer coating on the substrate surface. The fabrication process is simple and yields thin coatings characterized by high optical transparency and large electrical piezoresitivity. Such properties envisage potential applications of this polymer-supported coating for use in strain sensing. The electrical and mechanical properties of these PMMA/graphene coatings were characterized by bending tests. The electrical transport was investigated as a function of the applied stress. The structural and strain properties of the polymer composite material were studied under stress by infrared thermography and micro-Raman spectroscopy.
ABSTRACT
The present work is concerned with the use of a quantum well infrared photodetector (QWIP) infrared camera to measure very small temperature variations, which are related to thermoelastic/plastic effects, developing on composites under relatively low loads, either periodic or due to impact. As is evident from previous work, some temperature variations are difficult to measure, being at the edge of the IR camera resolution and/or affected by the instrument noise. Conversely, they may be valuable to get either information about the material characteristics and its behavior under periodic load (thermoelastic), or to assess the overall extension of delaminations due to impact (thermo-plastic). An image post-processing procedure is herein described that, with the help of a reference signal, allows for suppression of the instrument noise and better discrimination of thermal signatures induced by the two different loads.