Bulk elastic fingering instability in Hele-Shaw cells.

We demonstrate experimentally the existence of a purely elastic, nonviscous fingering instability which arises when air penetrates into an elastomer confined in a Hele-Shaw cell. Fingers appear sequentially and propagate within the bulk of the material as soon as a critical strain, independent of the elastic modulus, is exceeded. Key elements in the driving force of the instability are the confinement of the gel and its adhesion to the plates of the cell, which result in a considerable expense of elastic energy during the growth of the air bubble.

Evidence of deep water penetration in silica during stress corrosion fracture.

We measure the thickness of the heavy water layer trapped under the stress corrosion fracture surface of silica using neutron reflectivity experiments. We show that the penetration depth is 65-85   Å, suggesting the presence of a damaged zone of ∼100   Šextending ahead of the crack tip during its propagation. This estimate of the size of the damaged zone is compatible with other recent results.

Effects of finite probe size on self-affine roughness measurements.

The roughness of fracture surfaces exhibits self-affinity for a wide variety of materials and loading conditions. The universality and the range of scales over which this regime extends are still debated. The topography of these surfaces is however often investigated with a finite contact probe. In this case, we show that the correlation function of the roughness can only be measured down to a length scale Deltax{c} which depends on the probe size R, the Hurst exponent zeta of the surface and its topothesy l, and exhibits spurious behavior at smaller scales. First, we derive the dependence of Deltax{c} on these parameters from a simple scaling argument. Then, we verify this dependence numerically. Finally, we establish the relevance of this analysis from AFM measurements on an experimental glass fracture surface and provide a metrological procedure for roughness measurements.

Plasticity-induced structural anisotropy of silica glass.

Amorphous silica density at ambient pressure is known to depend on thermal history (through the quenching rate) but also, at room temperature, on the maximum pressure applied in the past. Here we show that beyond density, a mechanical loading can endow the structure with an orientational order. Molecular dynamics simulations show evidence that amorphous silica develops a permanent anisotropic structure after extended shear plastic flow. This anisotropy which survives for an unstressed specimen is revealed markedly by the fabric tensor computed over the Si-O-Si orientations, albeit the SiO4 tetrahedra microstructure remains mostly unaltered.

Scaling exponents for fracture surfaces in homogeneous glass and glassy ceramics.

We investigate the scaling properties of postmortem fracture surfaces in silica glass and glassy ceramics. In both cases, the 2D height-height correlation function is found to obey Family-Viseck scaling properties, but with two sets of critical exponents, in particular, a roughness exponent zeta approximately 0.75 in homogeneous glass and zeta approximately 0.4 in glassy ceramics. The ranges of length scales over which these two scalings are observed are shown to be below and above the size of the process zone, respectively. A model derived from linear elastic fracture mechanics in the quasistatic approximation succeeds to reproduce the scaling exponents observed in glassy ceramics. The critical exponents observed in homogeneous glass are conjectured to reflect the damage screening occurring for length scales below the size of the process zone.

Two-dimensional scaling properties of experimental fracture surfaces.

The self-affine properties of postmortem fracture surfaces in silica glass and aluminum alloy were investigated through the 2D height-height correlation function. They are observed to exhibit anisotropy. The roughness, dynamic, and growth exponents are determined and shown to be the same for the two materials, irrespective of the crack velocity. These exponents are conjectured to be universal.

Glass breaks like metal, but at the nanometer scale.

We report in situ atomic force microscopy experiments which reveal the presence of nanoscale damage cavities ahead of a stress-corrosion crack tip in glass. Their presence might explain the departure from linear elasticity observed in the vicinity of a crack tip in glass. Such a ductile fracture mechanism, widely observed in the case of metallic materials at the micrometer scale, might be also at the origin of the striking similarity of the morphologies of fracture surfaces of glass and metallic alloys at different length scales.

Scaling of crack surfaces and implications for fracture mechanics

The scaling laws describing the roughness development of crack surfaces are incorporated into the Griffith criterion. We show that, in the case of a Family-Vicsek scaling, the energy balance leads to a purely elastic brittle behavior. On the contrary, it appears that an anomalous scaling reflects an R-curve behavior associated with a size effect of the critical resistance to crack growth in agreement with the fracture process of heterogeneous brittle materials exhibiting a microcracking damage.