1.
RSC Adv
; 11(47): 29870-29876, 2021 Sep 01.
Article
in English
| MEDLINE
| ID: mdl-35479571
ABSTRACT
Fast (60 kHz) magic angle spinning solid-state NMR allows very sensitive proton detection in highly paramagnetic organometallic powders. We showcase this technique with the complete assignment of 1H and 13C resonances in a high-spin Fe(ii) polymerisation catalyst with less than 2 mg of sample at natural abundance.
