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J Dent ; 37(12): 923-31, 2009 Dec.
Article in English | MEDLINE | ID: mdl-19660517

ABSTRACT

OBJECTIVES: This study examined the effect of saliva contamination on the microtensile bond strength (microTBS) of resin luting cements to dentin. METHODS: For RelyX ARC (ARC, 3M ESPE), dentin surfaces were etched with 32% phosphoric acid. The subgroups were: ARC-control (uncontaminated), ARC-I (saliva contamination, blot-dried), ARC-II (saliva contamination, rinse, blot-dried) and ARC-III (saliva contamination, rinse, re-etch, rinse, blot-dried). For Panavia F 2.0 (PF, Kuraray), the subgroups were: PF-control (uncontaminated), PF-I (saliva contamination, dried), PF-II (saliva contamination, rinse, dried), PF-III (primer, saliva contamination, dried), PF-IV (primer, saliva contamination, dried, primer re-applied) and PF-V (primer, saliva contamination, rinse, dried, primer re-applied). Composite blocks were luted onto dentin using the two cements. Bonded specimens were sectioned into 0.9 mm x 0.9 mm beams for muTBS testing. Representative fractured beams were prepared for fractographic analysis. RESULTS: For ARC, salivary contamination of etched dentin (ARC-I) significantly lowered bond strength (p=0.001). Rinsing saliva off with water (ARC-II) restored bond strength to control level. Re-etching dentin surface after rinsing (ARC-III) resulted in the lowest bond strength (p<0.001). For PF, salivary contamination of dentin before (PF-I) and after application of primer (PF-III and PF-IV) significantly lowered bond strength (p<0.001). Rinsing saliva off with water and re-application of primer (PF-II and PF-V) improved bond strength. CONCLUSION: Saliva contamination during luting deteriorated the bond quality of resin cements. Decontamination by rinsing with water was most effective in restoring the bond strength of RelyX ARC. Decontamination by water-rinsing and primer re-application after rinsing improved the bond strength of Panavia F 2.0.


Subject(s)
Dental Bonding , Dentin/ultrastructure , Resin Cements/chemistry , Saliva/physiology , Acid Etching, Dental/methods , Adhesiveness , Bisphenol A-Glycidyl Methacrylate/chemistry , Carbon Compounds, Inorganic/chemistry , Dental Cements/chemistry , Dental Stress Analysis , Dentin-Bonding Agents/chemistry , Humans , Materials Testing , Methacrylates/chemistry , Phosphoric Acids/chemistry , Polyethylene Glycols/chemistry , Polymethacrylic Acids/chemistry , Polyurethanes/chemistry , Silicon Compounds/chemistry , Stress, Mechanical , Surface Properties , Tensile Strength , Water/chemistry
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