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Angew Chem Int Ed Engl ; 62(52): e202313659, 2023 Dec 21.
Article in English | MEDLINE | ID: mdl-37966018

ABSTRACT

We report the first reductive vinylation of alkyl iodides. The reaction uses a vinyl thianthrenium salt, a palladium catalyst, and an alkyl zinc intermediate formed in situ to trap the Ln PdII (vinyl) complex formed after oxidative addition before it undergoes undesired homocoupling to form butadiene.

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