Influence of Subsequently Applied Mechanical and Thermal Loads on Surfaces Ground with Mechanical Main Impact.

To generate advanced properties for the wear resistance and fatigue life of components and allow for an improved, application-oriented development of part specifications, a precisely tailored initial machining or manufacturing process is necessary. In addition, it is important to know how subsequent machining steps or operational loads affect the components' condition. Residual stresses are a meaningful measurand for evaluating the modifications that a machining process induces into the material. The desired modifications should be specified regarding the final state for the required operational behavior. Thus, the stability of the modifications can be considered so that they can be beneficial in service. This investigation is part of fundamental research in the field of the Collaborative Research Center (CRC) "Process Signatures". By applying defined selected loads, the effects on machined surface layers are investigated since machined components are exposed to further loads during use. For this reason, experimental process chains are applied in this work to grind-strengthened specimens as possible application cases and corresponding loads. These experimental process chains consist of defined mechanical and thermal loads, which are applied to the specimens using a thermal and mechanical testing system. Furthermore, it is investigated how these additional loads affect the modifications previously introduced by the grinding process. The influence of the additional loads is evaluated by using radiographic and electron microscopic examinations. It can be observed that the sequence, as well as the type of the applied loads, play a significant role in the development of the modifications.

Short-Term Characterization of Spherical 100Cr6 Steel Samples Using Micro Compression Test.

For the establishment of a novel development process of new structural materials, short-term characterization methods capable of testing hundreds of spherical micro samples are needed. This paper introduces a compression test on spherical micro samples as a short-term characterization method to investigate the elastic-plastic deformation behavior. To demonstrate the potential of this newly developed method, the micro compression test is performed with a maximum loading of 300 N on 100Cr6 (AISI 52100 bearing steel) samples, with a diameter of 0.8 mm, in 15 different heat treatment conditions. The austenitizing temperature is varied between 800 and 1150 °C. Tempering of the samples is carried out in a differential scanning calorimetry process with temperatures of 180, 230 and 300 °C. Out of force-displacement curves and stress-strain relations, so-called descriptors (characteristic values) which are sensitive to the applied heat treatment can be extracted. The change of mechanical properties due to heat treatment and the resulting microstructure is presented by the trend of a stress descriptor in dependence of austenitizing and annealing temperature, which can be compared to the trend of the tensile strength as a material property obtained by conventional tensile tests. The trend of the descriptor determined in the compression test on spherical samples indicates the validity of this approach as a short-term characterization method.

Descriptors for High Throughput in Structural Materials Development.

The development of novel structural materials with increasing mechanical requirements is a very resource-intense process if conventional methods are used. While there are high-throughput methods for the development of functional materials, this is not the case for structural materials. Their mechanical properties are determined by their microstructure, so that increased sample volumes are needed. Furthermore, new short-time characterization techniques are required for individual samples which do not necessarily measure the desired material properties, but descriptors which can later be mapped on material properties. While universal micro-hardness testing is being commonly used, it is limited in its capability to measure sample volumes which contain a characteristic microstructure. We propose to use alternative and fast deformation techniques for spherical micro-samples in combination with classical characterization techniques such as XRD, DSC or micro magnetic methods, which deliver descriptors for the microstructural state.